1,2,5,6-四溴环辛烷合成路线 (共 8 条)
反应条件
pyridinium tribromide in methanol
参考文献
Eglinton,G. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 474 - 479
反应条件
tetrachloromethane; bromine
参考文献
Detert, Heiner; Rose, Bernd; Mayer, Winfried; Meier, Herbert
Chemische Berichte, 1994 , vol. 127, # 8 p. 1529 - 1532
反应条件
1: sodium; ethanol 2: tetrachloromethane; bromine View Scheme
参考文献
Jones
Journal of the Chemical Society, 1954 , p. 312,316
反应条件
18-crown-6 ether; potassium tert-butylate in water; pentane
参考文献
Detert, Heiner; Rose, Bernd; Mayer, Winfried; Meier, Herbert
Chemische Berichte, 1994 , vol. 127, # 8 p. 1529 - 1532
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in hexane Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Davila, Alfonso; Ramezanian, Merrikh S.; Fronczek, Frank R.; McLaughlin, Mark L.
Tetrahedron Letters, 1996 , vol. 37, # 15 p. 2517 - 2520
反应条件
18-crown-6 ether; potassium tert-butylate 1.) THF, 0 deg C, 2 h, 2.) pentane, H2O, 36 deg C, 2-3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Detert, Heiner; Rose, Bernd; Mayer, Winfried; Meier, Herbert
Chemische Berichte, 1994 , vol. 127, # 8 p. 1529 - 1532
反应条件
poly(styrylmethylthiol); sodium methylate in tetrahydrofuran; methanol T=50°C; 5 h; Yield given;
参考文献
Tetrahedron Letters, , vol. 24, # 36 p. 3913 - 3916
反应条件
poly(styrylmethylthiol); sodium methylate in tetrahydrofuran; methanol T=50°C; 5 h; Yield given;
参考文献
Janout, Vaclav; Cefelin, Pavel
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3913 - 3916