4-氧代-4-(2,4,5-三甲氧基苯基)丁酸合成路线 （共 5 条）
反应条件
carbon disulfide; aluminium trichloride
参考文献
Ameer, Farouk; Giles, Robin G. F.; Green, Ivan R.; Pearce, Rene
Synthetic Communications, 2004 , vol. 34, # 7 p. 1247 - 1258
参考文献
Bargellini; Giua
Gazzetta Chimica Italiana, 1912 , vol. 42 I, p. 205
反应条件
1: Zn; HCl / toluene 2: PPA View Scheme
参考文献
Brunner; Hanke
Monatshefte fuer Chemie, 1954 , vol. 85, p. 88,91
反应条件
1: 62 percent / amalgameted Zn, 6N HCl / 5.5 h / Heating 2: 12.3 g / polyphosphoric acid / 3 h / 90 - 100 °C 3: 84 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 8 h / Heating View Scheme
参考文献
Matsumoto, Takeshi; Ichihara, Akitami; Yanagiya, Mitsutoshi; Yuzawa, Tamio; Sannai, Akiyoshi; et al.
Helvetica Chimica Acta, 1985 , vol. 68, p. 2324 - 2331
反应条件
1: N2H4+H2O; KOH / 190 °C
2: PCl5; benzene / anschliessend mit SnCl4
3: palladium/charcoal; mesitylene
View Scheme
参考文献
Brunner; Hanke
Monatshefte fuer Chemie, 1954 , vol. 85, p. 88,91
