4-氯-N-(2-羟基苯基)苯甲酰胺合成路线 (共 8 条)
反应条件
1: 2-chloro-5-carboxybenzene With 2,4,6-trichloro-1,3,5-triazine in dichloromethane T=40°C; 0.166667 h; Microwave irradiationSealed tube; 2: 2-amino-phenol in dichloromethane T=60°C; 0.5 h; Microwave irradiationSealed tube;
参考文献
Tetrahedron, , vol. 69, # 2 p. 791 - 795
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine in N,N-dimethyl acetamide T=120°C; P=4654.3 Torr; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 57, # 10 p. 2883 - 2887
反应条件
indium; acetic acid in tetrahydrofuran; water T=20°C; 0.5 h; Inert atmosphere;
参考文献
Lee, Hyejeong; Kim, Minki; Jun, Young Moo; Kim, Byeong Hyo; Lee, Byung Min
Heteroatom Chemistry, 2011 , vol. 22, # 2 p. 158 - 167
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate in N,N-dimethyl-formamide T=90°C; P=760 Torr;
参考文献
Journal of Chemical Research - Part S, , # 6 p. 235 - 237
反应条件
in dichloromethane T=0°C;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 11 p. 3141 - 3148
反应条件
1: triethylamine / dichloromethane / 1 h / 20 °C 2: indium; acetic acid / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Heteroatom Chemistry, , vol. 22, # 2 p. 158 - 167
反应条件
T=160°C; 0.166667 h; microwave-irradiation;
参考文献
Tetrahedron Letters, , vol. 49, # 29-30 p. 4464 - 4466
反应条件
Al3+ exchanged K10 clay in anhydrous xylene
T=140°C; 16 h; Green chemistry;
参考文献
Suresh, Dhanusu; Dhakshinamoorthy, Amarajothi; Pitchumani, Kasi
Tetrahedron Letters, 2013 , vol. 54, # 48 p. 6415 - 6419