(S)-(-)-4-异丁基氧氮杂环戊烷-2,5-二酮合成路线 (共 34 条)
反应条件
in tetrahydrofuran T=20°C; 16 h;
参考文献
Gerlach, Arne; Geller, Thomas
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 9-10 p. 1247 - 1249
反应条件
carbon in tetrahydrofuran T=55°C; 0.5 h;
参考文献
Milo, Anat; Neumann, Ronny
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 13 p. 2159 - 2165
参考文献
Bioresearch, Inc.
Patent: US5028693 A1, 1991 ;
反应条件
in tetrahydrofuran T=50°C;
参考文献
Zhang, Guolin; Liang, Fang; Song, Ximing; Liu, Daliang; Li, Mengjiang; Wu, Qiuhua
Carbohydrate Polymers, 2010 , vol. 80, # 3 p. 885 - 890
反应条件
thionyl chloride in tetrahydrofuran T=40°C; 4 h; Inert atmosphere;
参考文献
Xu, Xianghui; Yuan, Hui; Chang, Jing; He, Bin; Gu, Zhongwei
Angewandte Chemie - International Edition, 2012 , vol. 51, # 13 p. 3130 - 3133
反应条件
phosphorus tribromide in diethyl ether
参考文献
Itoh, Osamu; Honnami, Toshiya; Amano, Akira; Murata, Kouichi; Koichi, Youta; Sugita, Toshio
Journal of Organic Chemistry, 1992 , vol. 57, # 28 p. 7334 - 7338
反应条件
in tetrahydrofuran T=60°C; 4 h;
参考文献
Nagai, Atsushi; Sato, Daisuke; Ishikawa, Junichi; Ochiai, Bungo; Kudo, Hiroto; Endo, Takeshi
Macromolecules, 2004 , vol. 37, # 7 p. 2332 - 2334
反应条件
phosphorus tribromide in tetrachloromethane
参考文献
Chemische Berichte, , vol. 104, p. 3146 - 3155
反应条件
in benzene T=60 - 70°C; 0.25 h;
参考文献
Heterocycles, , vol. 64, p. 129 - 141
反应条件
1: triethylamine / acetonitrile / 4 h / 20 °C 2: H2 / Pd / acetic acid; 2-methyl-propan-2-ol; H2O View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 9 p. 2705 - 2707