1,3,5-三氯-2,4,6-三氟苯合成路线 （共 27 条）
反应条件
potassium fluoride in sulfolane T=190°C; 200 h;
参考文献
Chambers, Richard D.; Edwards, Andrew R.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 24 p. 3623 - 3627
反应条件
tetrachloromethane; chlorine T=200°C; Photolysis;
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
1: iron; aqueous NH4Cl 3: sulfuryl chloride; disulfur dichloride; aluminium chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
1: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 2: iron; aqueous NH4Cl 4: sulfuryl chloride; disulfur dichloride; aluminium chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
2: sulfuryl chloride; disulfur dichloride; aluminium chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
1: H2SO4; HNO3 2: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 3: iron; aqueous NH4Cl 5: sulfuryl chloride; disulfur dichloride; aluminium chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
disulfur dichloride; aluminium trichloride; sulfuryl dichloride
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
potassium fluoride Product distribution / selectivity;
参考文献
BASF Aktiengesellschaft
Patent: WO2006/111583 A1, 2006 ;
Location in patent: Page/Page column 10-11 ;
反应条件
2,4-di-Nitrobenzene; potassium fluoride in 1-methyl-pyrrolidin-2-one T=180°C; P=405.041 Torr; 16 h; Product distribution / selectivity;
参考文献
WO2006/111583 A1, ;
Page/Page column 10 ;
反应条件
potassium fluoride; tetrakis(diethylamino)phosphonium bromide T=180°C; 24 h; Product distribution / selectivity;
参考文献
BASF Aktiengesellschaft
Patent: WO2006/111583 A1, 2006 ;
Location in patent: Page/Page column 10 ;
