2-氯-N-(4-氯苯基)苯甲酰胺合成路线 (共 7 条)
参考文献
Zhang, Guofu; Zhao, Xiaobao; Yan, Yunbing; Ding, Chengrong
European Journal of Organic Chemistry, 2012 , # 4 p. 669 - 672
反应条件
di-tert-butyl peroxide in chlorobenzene T=110°C; 48 h; Further byproducts given;
参考文献
Leardini, Rino; Tundo, Antonio; Zanardi, Giuseppe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3164 - 3167
反应条件
1: thionyl chloride / 5 h / Reflux 2: triethylamine / ethyl acetate / 1 h / 0 - 20 °C View Scheme
参考文献
Zhang, Guofu; Zhao, Xiaobao; Yan, Yunbing; Ding, Chengrong
European Journal of Organic Chemistry, 2012 , # 4 p. 669 - 672
反应条件
phosphorus trichoride T=120°C;
参考文献
Hirwe; Jadhav; Sukhtankar
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, 1938 , vol. 7/, p. 216
反应条件
sulfuryl dichloride; benzene
参考文献
Hirwe; Jadhav; Sukhtankar
Journal of the Indian Chemical Society, 1939 , vol. 16, p. 281,284
反应条件
in cyclohexane 1 h; Irradiation;
参考文献
Grimshaw, James; Silva, A. Prasanna de
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 857 - 866
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 0 °C / Inert atmosphere
1.2: 2 h / 0 - 20 °C / Inert atmosphere
2.1: di-μ-chlorobis [5-hydroxy-2-[1-(hydroxyimino)ethyl]phenyl]palladium(II) dimer; potassium carbonate / N,N-dimethyl acetamide / 72 h / 140 °C / Inert atmosphere
View Scheme
参考文献
Zhang, Guofu; Zhao, Xiaobao; Yan, Yunbing; Ding, Chengrong
European Journal of Organic Chemistry, 2012 , # 4 p. 669 - 672