2’,3’,5’-三乙酰肌苷合成路线 （共 38 条）
参考文献
Patching, Simon G.; Baldwin, Stephen A.; Baldwin, Alexander D.; Young, James D.; Gallagher, Maurice P.; Henderson, Peter J. F.; Herbert, Richard B.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 3 p. 462 - 470
反应条件
sodium hydride in acetonitrile T=60°C; 4 h; Inert atmosphere;
参考文献
Mola, Laura; Font, Joan; Bosch, Lluis; Caner, Joaquim; Costa, Anna M.; Etxebarria-Jardi, Gorka; Pineda, Oriol; De Vicente, David; Vilarrasa, Jaume
Journal of Organic Chemistry, 2013 , vol. 78, # 12 p. 5832 - 5842
反应条件
sodium hydride in tetrahydrofuran T=20°C; 2 h; Inert atmosphere;
参考文献
Mola, Laura; Font, Joan; Bosch, Lluis; Caner, Joaquim; Costa, Anna M.; Etxebarria-Jardi, Gorka; Pineda, Oriol; De Vicente, David; Vilarrasa, Jaume
Journal of Organic Chemistry, 2013 , vol. 78, # 12 p. 5832 - 5842
反应条件
triethylamine in dichloromethane 22 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 53, # 9 p. 1887 - 1894
反应条件
potassium hydroxide; 15NH4Cl; triethylamine in acetonitrile 16 h;
参考文献
Chemical Communications, , # 31 p. 3968 - 3970
反应条件
hydrogen; palladium on activated charcoal P=3102.9 Torr; 16 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 2 p. 1769 - 1770
反应条件
1: 1.) Et3N; 2.) PPh3, diethyl azodicarboxylate; 3.) 80 percent HOAc / 1.) 100 deg C, 2 h; 2.) dioxane, 80 deg C, 6 h; 3.) 80 deg C 3: 95 percent / CF3SO3SiMe3 / acetonitrile / reflux, 1h; rt, 16 h 4: 1,8-diazabicyclo<5.4.0>undec-7-ene / acetonitrile 5: hydrogen / Pd/C / 16 h / 3102.9 Torr / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 2 p. 1769 - 1770
反应条件
2: 95 percent / CF3SO3SiMe3 / acetonitrile / reflux, 1h; rt, 16 h 3: 1,8-diazabicyclo<5.4.0>undec-7-ene / acetonitrile 4: hydrogen / Pd/C / 16 h / 3102.9 Torr / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 2 p. 1769 - 1770
反应条件
1: 95 percent / CF3SO3SiMe3 / acetonitrile / reflux, 1h; rt, 16 h 2: 1,8-diazabicyclo<5.4.0>undec-7-ene / acetonitrile 3: hydrogen / Pd/C / 16 h / 3102.9 Torr / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 2 p. 1769 - 1770
反应条件
1: 1,8-diazabicyclo<5.4.0>undec-7-ene / acetonitrile 2: hydrogen / Pd/C / 16 h / 3102.9 Torr / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 2 p. 1769 - 1770
