1-甲基-3-(三氟乙酰基)-1H-吲哚合成路线 （共 11 条）
参考文献
Hassinger, Heidi L.; Soll, Richard M.; Gribble, Gordon W.
Tetrahedron Letters, 1998 , vol. 39, # 20 p. 3095 - 3098
反应条件
potassium carbonate; methyl iodide in dichloromethane; water; acetone
参考文献
Monsanto Company
Patent: US5994270 A1, 1999 ;
反应条件
dimethylsulfide; boron trifluoride in dichloromethane -78 deg C to r.t.;
参考文献
Kiselyov, Alexander S.
Tetrahedron Letters, 1995 , vol. 36, # 23 p. 4005 - 4008
反应条件
1: copper(l) chloride; sodium nitrite; hydrogenchloride / 1,2-dichloro-ethane / 7 h / 0 - 80 °C / |Schlenk technique; |Inert atmosphere 2: 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); potassium carbonate / acetone / -78 - 20 °C / |Inert atmosphere View Scheme
参考文献
Wang, Shuai; Nie, Jing; Zheng, Yan; Ma, Jun-An
Organic Letters, 2014 , vol. 16, # 6 p. 1606 - 1609
反应条件
in diethyl ether 16 h; Ambient temperature;
参考文献
Biswas; Mallik, Haimanti; Saha, Aparna
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 9 p. 841 - 843
反应条件
dimethyl-(4-nitro-buta-1,3-dienyl)-amine 12 h; Ambient temperature;
参考文献
Takeuchi, Naoki; Tanabe, Mitsuharu; Hagiwara, Masanori; Goto, Kaori; Koike, Takeshi; Tobinaga, Seisho
Heterocycles, 1994 , vol. 38, # 3 p. 613 - 628
反应条件
1: 87 percent / 0 °C 2: 85 percent / NaH View Scheme
参考文献
Whalley
Journal of the Chemical Society, 1954 , p. 1651
反应条件
trifluoroacetic acid 12 h; Ambient temperature;
参考文献
Takeuchi, Naoki; Tanabe, Mitsuharu; Hagiwara, Masanori; Goto, Kaori; Koike, Takeshi; Tobinaga, Seisho
Heterocycles, 1994 , vol. 38, # 3 p. 613 - 628
反应条件
in diethyl ether 16 h; Ambient temperature;
参考文献
Biswas; Mallik, Haimanti; Saha, Aparna
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 9 p. 841 - 843
反应条件
hydrogenchloride; diethyl ether; zinc(II) chloride Behandeln des Reaktionsgemisches mit Wasser;
参考文献
Whalley
Journal of the Chemical Society, 1954 , p. 1651
