4,5-二甲基-1,2-苯二胺合成路线 （共 140 条）
反应条件
in butan-1-ol 12 h; Heatingxylene, 4 h, reflux;
参考文献
Tetrahedron Letters, , vol. 28, # 13 p. 1389 - 1392
参考文献
Tetrahedron Letters, , vol. 28, # 13 p. 1389 - 1392
反应条件
hydrogenchloride
24 h; Heating;
参考文献
Essassi, E. M.; Lamkadem, A.; Zniber, R.
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 3 p. 277 - 286
反应条件
1: hydrogenchloride / water / 6 h / |Reflux
2: tetrabutylammomium bromide; potassium hydroxide / tetrahydrofuran / 0 °C
3: Dess-Martin periodane / dichloromethane / 6 h / 0 °C
View Scheme
参考文献
Eom, Young Woo; Oh, Sangtae; Woo, Ho Bum; Ham, Jungyeob; Ahn, Chan Mug; Lee, Seokjoon
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 4 p. 1272 - 1274
反应条件
1: PhNSO / toluene / |Reflux
2: bromine; iodine / dichloromethane
View Scheme
参考文献
Park, Jin Su; Jin, Sung-Ho; Gal, Yeong-Soon; Lee, Jun Hee; Lee, Jae Wook
Molecular Crystals and Liquid Crystals, 2012 , vol. 567, # 1 p. 102 - 109,8
反应条件
acetic acid in benzene
T=20°C; 24 h; Inert atmosphere;
参考文献
Conda-Sheridan, Martin; Marler, Laura; Park, Eun-Jung; Kondratyuk, Tamara P.; Jermihov, Katherine; Mesecar, Andrew D.; Pezzuto, John M.; Asolkar, Ratnakar N.; Fenical, William; Cushman, Mark
Journal of Medicinal Chemistry, 2010 , vol. 53, # 24 p. 8688 - 8699
反应条件
hydrogenchloride
2.5 h; Heating;
参考文献
Essassi, E. M.; Lamkadem, A.; Zniber, R.
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 3 p. 277 - 286
反应条件
in benzene
5 h; Heating;
参考文献
Merchan; Garin; Tejero
Synthesis, 1982 , vol. No. 11, p. 984 - 986
反应条件
in benzene
5 h; Heating;
参考文献
Merchan; Garin; Tejero
Synthesis, 1982 , vol. No. 11, p. 984 - 986
反应条件
in benzene
5 h; Heating;
参考文献
Merchan; Garin; Tejero
Synthesis, 1982 , vol. No. 11, p. 984 - 986
