4,5-二甲基-1,2-苯二胺合成路线 （共 140 条）
反应条件
in ethanol; water 2 h; Heating;
参考文献
Leeson, Paul D.; Baker, Raymond; Carling, Robert W.; Curtis, Neil R.; Moore, Kevin W.; et al.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 4 p. 1243 - 1252
反应条件
in ethanol 2 h; Heating;
参考文献
Kazimierczuk; Pfleiderer
1982 , vol. No. 4, p. 754 - 761
反应条件
1: 79 percent / ethanol / 3 h 2: 94 percent / POCl3 / 2 h / Heating View Scheme
参考文献
Alphonse, France-Aimee; Karim, Rehana; Cano-Soumillac, Celine; Hebray, Marielle; Collison, David; Garner, C. David; Joule, John A.
Tetrahedron, 2005 , vol. 61, # 46 p. 11010 - 11019
反应条件
selenium(IV) oxide chloride in toluene 10 h; Heating;
参考文献
Roesky, Herbert W.; Weber, Karl-Ludwig; Seseke, Ulrich; Pinkert, Waltraud; Noltemeyer, Mathias; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1985 , p. 565 - 572
反应条件
in methanol; water T=50°C; 1 h;
参考文献
Frei, Reto; Breitbach, Anthony S.; Blackwell, Helen E.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 21 p. 5226 - 5229
反应条件
gallium trifluoromethanesulfonate T=20°C; 0.1 h;
参考文献
Liu, Juyan; Liu, Qian; Xu, Wei; Wang, Weilu
Chinese Journal of Chemistry, 2011 , vol. 29, # 8 p. 1739 - 1744
反应条件
tetrabutyl-ammonium chloride in water; toluene T=160°C; 0.166667 h; Microwave irradiation;
参考文献
Karuvalam, Ranjith P.; Haridas, Karickal R.; Shetty, Suchetha N.
Journal of the Chilean Chemical Society, 2012 , vol. 57, # 2 p. 1122 - 1125,4
反应条件
RuCl2(dppe)2; hydrogen T=120°C; P=112511 Torr; 40 h; Green chemistry;
参考文献
Yu, Bo; Zhang, Hongye; Zhao, Yanfei; Chen, Sha; Xu, Jilei; Huang, Changliang; Liu, Zhimin
Green Chemistry, 2013 , vol. 15, # 1 p. 95 - 99
反应条件
1.1: 82 percent / NaHCO3 / H2O; tetrahydrofuran / 12 h 2.1: 85 mg / H2 / Pd(OH)2 / methanol / 2 h 3.1: HCl / H2O 3.2: NaOH / H2O / 5 h / 20 °C / pH 7 - 8 View Scheme
参考文献
Maggio-Hall, Lori A.; Dorrestein, Pieter C.; Escalante-Semerena, Jorge C.; Begley, Tadhg P.
Organic Letters, 2003 , vol. 5, # 13 p. 2211 - 2213
反应条件
2-(n-morpholino)ethanesulfonic acid in water T=37°C; pH=6;
参考文献
Maggio-Hall, Lori A.; Dorrestein, Pieter C.; Escalante-Semerena, Jorge C.; Begley, Tadhg P.
Organic Letters, 2003 , vol. 5, # 13 p. 2211 - 2213
