1-(2-甲基-1-环戊烯基)乙酮合成路线 （共 47 条）
反应条件
aluminium trichloride in dichloromethane 24 h; Heating;
参考文献
Pardo, Roselyne; Santelli, Maurice
Tetrahedron Letters, 1981 , vol. 22, # 39 p. 3843 - 3846
反应条件
(i) ZnCl2, (ii) KOH; Multistep reaction;
参考文献
Hudlicky, Tomas; Kwart, Lawrence D.; Tiedje, Mark H.; Ranu, Brindaban C.; Short, Robert P.; et al.
Synthesis, 1986 , # 9 p. 716 - 727
反应条件
carbon disulfide; tin(IV) chloride T=0°C; Erhitzen des nach der Hydrolyse erhaltenen Reaktionsprodukts mit N,N-Dimethyl-anilin;
参考文献
Nenitzescu; Cantuniari
Chemische Berichte, 1932 , vol. 65, p. 1449,1453
Justus Liebigs Annalen der Chemie, 1934 , vol. 510, p. 128,142, 143
反应条件
aluminium trichloride; acetyl chloride 1.) CH2Cl2, 30 min, 2.) CH2Cl2, reflux, 5 h; Yield given. Multistep reaction;
参考文献
Morel-Fourrier, Christophe; Dulcere, Jean-Pierre; Santelli, Maurice
Journal of the American Chemical Society, 1991 , vol. 113, # 21 p. 8062 - 8069
反应条件
aluminium trichloride; acetyl chloride 1.) CH2Cl2, 30 min, 2.) CH2Cl2, reflux, 4 h; Yield given. Multistep reaction;
参考文献
Morel-Fourrier, Christophe; Dulcere, Jean-Pierre; Santelli, Maurice
Journal of the American Chemical Society, 1991 , vol. 113, # 21 p. 8062 - 8069
反应条件
aluminium trichloride; acetyl chloride 1.) CH2Cl2, 30 min, 2.) CH2Cl2, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Morel-Fourrier, Christophe; Dulcere, Jean-Pierre; Santelli, Maurice
Journal of the American Chemical Society, 1991 , vol. 113, # 21 p. 8062 - 8069
反应条件
aluminium trichloride; acetyl chloride 1.) CH2Cl2, 30 min, 2.) CH2Cl2, reflux, 10 h; Yield given. Multistep reaction;
参考文献
Morel-Fourrier, Christophe; Dulcere, Jean-Pierre; Santelli, Maurice
Journal of the American Chemical Society, 1991 , vol. 113, # 21 p. 8062 - 8069
反应条件
aluminium trichloride; acetyl chloride 1.) CH2Cl2, 30 min, 2.) CH2Cl2, reflux, 3.5 h; Yield given. Multistep reaction;
参考文献
Morel-Fourrier, Christophe; Dulcere, Jean-Pierre; Santelli, Maurice
Journal of the American Chemical Society, 1991 , vol. 113, # 21 p. 8062 - 8069
反应条件
1: 78 percent / 10percent HBF4 / tetrahydrofuran / Ambient temperature 2: 70 percent / 10percent HBF4, HgO / tetrahydrofuran / Ambient temperature 4: tetrahydrofuran / -78 °C View Scheme
参考文献
Dieter, R. Karl; Jenkitkasemwong, Yawares
Tetrahedron Letters, 1982 , vol. 23, # 37 p. 3747 - 3750
反应条件
1: 69 percent 2: 78 percent / 10percent HBF4 / tetrahydrofuran / Ambient temperature 3: 70 percent / 10percent HBF4, HgO / tetrahydrofuran / Ambient temperature 5: tetrahydrofuran / -78 °C View Scheme
参考文献
Dieter, R. Karl; Jenkitkasemwong, Yawares
Tetrahedron Letters, 1982 , vol. 23, # 37 p. 3747 - 3750
