1-(2-甲基-1-环戊烯基)乙酮合成路线 （共 47 条）
反应条件
toluene-4-sulfonic acid T=60 - 80°C; cyclocondensation; P=0.0150015 Torr; 0.25 h;
参考文献
Bouillon, Jean-Philippe; Portella, Charles; Bouquant, James; Humbel, Stephane
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5823 - 5830
反应条件
water; hafnium tetrachloride; butan-1-ol; [Ir(1,5-cyclooctadiene)2]PF6; methyl-ethyl phosphite T=70°C; 15 h;
参考文献
Hirabayashi, Tomotaka; Okimoto, Yoshio; Saito, Akiyo; Morita, Masao; Sakaguchi, Satoshi; Ishii, Yasutaka
Tetrahedron, 2006 , vol. 62, # 10 p. 2231 - 2234
反应条件
aluminium trichloride in chloroform 1) 2h, reflux, 2) RT, 2 days,;
参考文献
Harding, Kenn E.; Clement, Katherine S.; Gilbert, John C.; Wiechman, Barry
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2049 - 2050
反应条件
hydrogen fluoride in acetonitrile T=25°C;
参考文献
Danheiser, Rick L.; Carini, David J.; Basak, Ajoy
Journal of the American Chemical Society, 1981 , vol. 103, # 6 p. 1604 - 1606
反应条件
formic acid T=100°C; 13.5 h;
参考文献
Menashe, Naim; Shvo, Youval
Journal of Organic Chemistry, 1993 , vol. 58, # 26 p. 7434 - 7439
反应条件
aluminium trichloride in dichloromethane T=-78 - 30°C; 5 h;
参考文献
Pardo, Roselyne; Santelli, Maurice
Tetrahedron Letters, 1981 , vol. 22, # 39 p. 3843 - 3846
反应条件
aluminium trichloride in dichloromethane 2 h; Heatingvar. alkanes and alkenes, var. acyl chlorides; Mechanism;
参考文献
Pardo, Roselyne; Santelli, Maurice
Tetrahedron Letters, 1981 , vol. 22, # 39 p. 3843 - 3846
反应条件
1: 1.) ZnI2, 2.)ZnCl2 grade / 1.) 0 deg C, 15 min, 2.) 0 deg C, 2 h 2: Al2O3 / CH2Cl2 / 12 h / Ambient temperature View Scheme
参考文献
Hudlicky, T.; Srnak, T.
Tetrahedron Letters, 1981 , vol. 22, # 35 p. 3351 - 3354
反应条件
zinc(II) chloride T=10 - 15°C; 10 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Beak,P.; Rogers,K.R.
Journal of the American Chemical Society, 1980 , vol. 102, p. 3848
反应条件
aluminum oxide 48 h; Ambient temperature;
参考文献
Zaidlewicz, Marek
Synthesis, 1988 , # 9 p. 701 - 703
