2-(4-溴苯基)-1,3-苯并噁唑合成路线 （共 35 条）
反应条件
copper(l) iodide; oxygen; palladium diacetate; potassium carbonate in 1,4-dioxane T=120°C; 48 h; Sealed tube;
参考文献
Zhang, Manli; Zhang, Shouhui; Liu, Miaochang; Cheng, Jiang
Chemical Communications, 2011 , vol. 47, # 41 p. 11522 - 11524
反应条件
palladium dichloride in chlorobenzene 4 h; Reflux;
参考文献
Xie, Hou-Zhi; Gao, Qi; Liang, Ying; Wang, Heng-Shan; Pan, Ying-Ming
Green Chemistry, 2014 , vol. 16, # 4 p. 2132 - 2135
反应条件
1: 99 percent / tetrahydrofuran / 24 h / 20 °C 2: 92 percent / CuI; Cs2CO3; 1,10-phenanthroline / 1,2-dimethoxy-ethane / 24 h / Heating View Scheme
参考文献
Semiconductor Energy Laboratory Co., Ltd.
Patent: US2012/178933 A1, 2012 ;
反应条件
1: 99 percent / tetrahydrofuran / 24 h / 20 °C 2: 92 percent / CuI; Cs2CO3; 1,10-phenanthroline / 1,2-dimethoxy-ethane / 24 h / Heating View Scheme
参考文献
Evindar, Ghotas; Batey, Robert A.
Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 1802 - 1808
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in ethylene glycol dimethyl ether 48 h; Heating;
参考文献
Viirre, Russell D.; Evindar, Ghotas; Batey, Robert A.
Journal of Organic Chemistry, 2008 , vol. 73, # 9 p. 3452 - 3459
反应条件
1: hydrazine hydrate; water / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere 2: dichloro bis(acetonitrile) palladium(II); sodium carbonate; copper diacetate; tetrabutylammomium bromide; 1,10-phenanthroline / dimethyl sulfoxide; 1,4-dioxane / 4.58 h / 20 - 100 °C / |Inert atmosphere View Scheme
参考文献
Yu, Xinzhang; Li, Xingwei; Wan, Boshun
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 37 p. 7479 - 7482
反应条件
1: 96 percent / ethanol / Heating 2: 100 percent / iodosobenzene diacetate / acetonitrile / Heating View Scheme
参考文献
Malakhova; Malakhov; Kuznitsova; Varnavskii; Kadutskii; Kozhich; Korshun; Berlin
Russian Journal of Bioorganic Chemistry, 1998 , vol. 24, # 9 p. 611 - 617
反应条件
1: 96 percent / ethanol / Heating 2: 100 percent / iodosobenzene diacetate / acetonitrile / Heating View Scheme
参考文献
Semiconductor Energy Laboratory Co., Ltd.
Patent: US2012/178933 A1, 2012 ;
反应条件
1: hydrazine / methanol; chloroform; water / 12 h / 20 °C 2: acetic acid / water / 0.5 h / 20 °C 3: oxygen; copper(II) bis(trifluoromethanesulfonate) / toluene / 3 h / 80 °C View Scheme
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
反应条件
1: acetic acid / water / 0.5 h / 20 °C 2: oxygen; copper(II) bis(trifluoromethanesulfonate) / toluene / 3 h / 80 °C View Scheme
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
