2-(4-溴苯基)-1,3-苯并噁唑合成路线 (共 35 条)
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in ethylene glycol dimethyl ether 24 h; Heating;
参考文献
Viirre, Russell D.; Evindar, Ghotas; Batey, Robert A.
Journal of Organic Chemistry, 2008 , vol. 73, # 9 p. 3452 - 3459
反应条件
Na8H[PW9O34]*7H2O in acetonitrile T=25°C; 6 h;
参考文献
Zhao, Shen; Chen, Yang; Song, Yu-Fei
Applied Catalysis A: General, 2014 , vol. 475, p. 140 - 146
反应条件
poly(ethylene glycol)-bound sulphonic acid in 1,4-dioxane; chloroform T=60 - 65°C;
参考文献
Chikhale, Rupesh V.; Pant, Amit M.; Menghani, Sunil S.; Wadibhasme, Pankaj G.; Khedekar, Pramod B.
South African Journal of Chemistry, 2013 , vol. 66, p. 254 - 262
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in ethylene glycol dimethyl ether 24 h; Heating;
参考文献
Bonnamour, Julien; Bolm, Carsten
Organic Letters, 2008 , vol. 10, # 13 p. 2665 - 2667
反应条件
oxygen; copper(II) bis(trifluoromethanesulfonate) in o-xylene T=140°C; P=760.051 Torr; 28 h;
参考文献
Ueda, Satoshi; Nagasawa, Hideko
Angewandte Chemie - International Edition, 2008 , vol. 47, # 34 p. 6411 - 6413
反应条件
1: With copper diacetate; palladium diacetate; trifluoroacetic acid in ethylene glycol dimethyl ether T=120°C; 24 h; Inert atmosphereSealed tube; 2: With potassium carbonate in ethylene glycol dimethyl ether; water T=20°C;
参考文献
Wang, Min; Li, Dengke; Zhou, Wei; Wang, Lei
Tetrahedron, 2012 , vol. 68, # 7 p. 1926 - 1930
反应条件
1,10-phenanthroline; palladium diacetate; caesium carbonate in dimethyl sulfoxide T=150°C; 20 h; Inert atmosphere;
参考文献
Yu, Peng; Zhang, Guangyou; Chen, Fan; Cheng, Jiang
Tetrahedron Letters, 2012 , vol. 53, # 34 p. 4588 - 4590
反应条件
1: in toluene RefluxGreen chemistry; 2: With trichlorophosphate in toluene RefluxGreen chemistry;
参考文献
Sung, Gi Hyeon; Lee, In-Hye; Kim, Bo Ram; Shin, Dong-Soo; Kim, Jeum-Jong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Tetrahedron, 2013 , vol. 69, # 17 p. 3530 - 3535
反应条件
oxygen; copper(II) bis(trifluoromethanesulfonate) in toluene T=80°C; 3 h;
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
反应条件
1: in 1,4-dioxane T=210°C; 0.25 h; 2: With sodium hydroxide in 1,4-dioxane; water
参考文献
SMITHKLINE BEECHAM CORPORATION
Patent: WO2007/88148 A1, 2007 ;
Location in patent: Page/Page column 27 ;