甲基-4,6-O-亚苄基-Α-D-吡喃葡糖苷合成路线 (共 91 条)
反应条件
calcium sulfate; benzaldehyde
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2412,2413
反应条件
oxygen; copper(l) chloride; palladium dichloride in water; N,N-dimethyl-formamide Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 53, # 51 p. 17501 - 17512
反应条件
zinc(II) chloride T=15°C;
参考文献
Patroni, Joseph J.; Stick, Robert V.
Australian Journal of Chemistry, 1985 , vol. 38, # 6 p. 947 - 952
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 10 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 39, # 8 p. 1983 - 1989
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; water T=20°C;
参考文献
Polish Journal of Chemistry, , vol. 79, # 2 p. 317 - 322
反应条件
1: With didodecanoyl peroxide in 1,2-dichloro-ethane 2 h; Inert atmosphereReflux; 2: With acetic acid in water; 1,2-dichloro-ethane 0.5 h; Inert atmosphere; 3: With tetrabutyl ammonium fluoride in water; 1,2-dichloro-ethane 1 h; Inert atmosphere; regioselective reaction;
参考文献
Attouche, Angie; Urban, Dominique; Beau, Jean-Marie
Angewandte Chemie - International Edition, 2013 , vol. 52, # 36 p. 9572 - 9575
Angew. Chem., 2013 , vol. 125, # 36 p. 9751 - 9754,4
反应条件
sodium ethanolate in ethanol 19 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 39, # 8 p. 1983 - 1989
反应条件
tetrabutyl ammonium fluoride in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 4 p. 744 - 753
反应条件
lithium hydroxide; dihydrogen peroxide in tetrahydrofuran T=0°C;
参考文献
Carbohydrate Research, , vol. 202, p. 67 - 79
反应条件
1: HCl 2: TsOH View Scheme
参考文献
Chemical Communications, , # 16 p. 1497 - 1498
Synlett, , vol. 1997, # 6 p. 669 - 670