甲基-4,6-O-亚苄基-Α-D-吡喃葡糖苷合成路线 (共 91 条)
反应条件
pyridinium p-toluenesulfonate in N,N-dimethyl-formamide
参考文献
Tatina, Madhubabu; Yousuf, Syed Khalid; Mukherjee, Debaraj
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 28 p. 5357 - 5360
反应条件
zinc(II) chloride T=12°C; 6 h;
参考文献
Kitagawa, Isao; Yoshikawa, Masayuki; Kobayashi, Katsuya; Imakura, Yasuhiro; Im, Kwang Sik; Ikenishi, Yuji
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 1 p. 296 - 300
反应条件
triethylsilane; copper(II) bis(trifluoromethanesulfonate) in dichloromethane; acetonitrile T=20°C; 0.5 h;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 45 p. 8662 - 8665
反应条件
titanium(IV) isopropylate; cyclohexylMgCl in tetrahydrofuran Ambient temperature;
参考文献
Lee, Jinhwa; Cha, Jin Kun
Tetrahedron Letters, 1996 , vol. 37, # 21 p. 3663 - 3666
反应条件
cyclohexene; palladium dihydroxide in ethanol 2 h; Heating;
参考文献
Hanessian, Stephen; Liak, Teng Jiam; Vanasse, Benoit
Synthesis, 1981 , # 5 p. 396 - 397
反应条件
camphor-10-sulfonic acid in chloroform Cyclization; Benzylidenation;
参考文献
Szolcsanyi, Peter; Gracza, Tibor; Koman, Marian; Pronayova, Naia; Liptaj, Tibor
Chemical Communications, 2000 , # 6 p. 471 - 472
反应条件
copper(II) bis(trifluoromethanesulfonate) in dichloromethane; acetonitrile T=20°C; 0.166667 h;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 45 p. 8662 - 8665
反应条件
VO(OTf)2 in dichloromethane; acetonitrile T=20°C; 0.166667 h;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 45 p. 8662 - 8665
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=60°C; P=250 Torr; 0.5 h; Yield given. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 278, # 1 p. 43 - 57
反应条件
1: methanol; D-glucopyranose With chloro-trimethyl-silane T=60°C; Fischer glycosidation; 5 h; 2: benzaldehyde dimethyl acetal With toluene-4-sulfonic acid in acetonitrile T=20°C;
参考文献
Izumi, Minoru; Fukase, Koichi; Kusumoto, Shoichi
Bioscience, Biotechnology and Biochemistry, 2002 , vol. 66, # 1 p. 211 - 214