N-(4-氯苯亚甲基)-4-甲苯磺酰胺合成路线 （共 24 条）
反应条件
potassium carbonate in acetonitrile
T=0 - 20°C; 24 h; Overall yield = 65 percent; enantioselective reaction;
参考文献
Illa, Ona; Namutebi, Mariam; Saha, Chandreyee; Ostovar, Mehrnoosh; Chen, C. Chun; Haddow, Mairi F.; Nocquet-Thibault, Sophie; Lusi, Matteo; McGarrigle, Eoghan M.; Aggarwal, Varinder K.
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 11951 - 11966
反应条件
1: C16H27Br10Ir2Sn2 / 1,2-dichloro-ethane / 0.42 h / 20 °C / |Inert atmosphere; |Schlenk technique
2: [Ir(COD)(SnCl3)Cl(μ-Cl)]2 / 1,2-dichloro-ethane / 2 h / 80 °C / |Schlenk technique; |Inert atmosphere
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参考文献
Chatterjee, Paresh Nath; Maity, Arnab Kumar; Mohapatra, Swapna Sarita; Roy, Sujit
Tetrahedron, 2013 , vol. 69, # 13 p. 2816 - 2826
反应条件
in tetrahydrofuran; diethyl ether
T=-5 - 0°C; 0.5 h; Inert atmosphere;
参考文献
Branco, Paula Serio; Raje, Vivek Prabhakar; Dourado, Jorge; Gordo, Joana
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 13 p. 2968 - 2974
反应条件
in 1,3,5-trimethyl-benzene
T=140°C; 12 h; Inert atmosphere; optical yield given as percent de;
参考文献
Yan, Yizhe; Xu, Kun; Fang, Yang; Wang, Zhiyong
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6849 - 6855
