反-3-羟基-β-硝基苯乙烯合成路线 （共 6 条）
反应条件
dimethylsulfide; boron trifluoride diethyl etherate in dichloromethane T=30°C; 1.5 h;
参考文献
Fuji; Kawabata; Fujita
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 12 p. 3662 - 3664
反应条件
CaO modified benzyl bromide T=102°C; Henry Nitro Aldol Condensation; 5 h;
参考文献
Research on Chemical Intermediates, , vol. 39, # 8 p. 3715 - 3725
反应条件
sodium hydroxide T=0°C;
参考文献
Chemische Berichte, , vol. 71, p. 2154,2161
反应条件
sulfuric acid; acetic acid Hydrogenation;
参考文献
Chemische Berichte, , vol. 71, p. 2154,2161
反应条件
in ethanol
3 h; Heating;
参考文献
Latif, N.; Mishriky, N.; Assad, F. M.; Meguid, S. Abdel
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 9 p. 872 - 874
反应条件
1: 2.) H2O / 1.)Et2O, room temp., 1-2 h, 2) 50-60 deg C, 4 h
2: butan-1-ol / 2 h / Heating
View Scheme
参考文献
Latif, Nazih; Assaad, Fahmy M.; Hosni, Hanaa
Liebigs Annalen der Chemie, 1987 , p. 495 - 498
