1-(3-氯苯基)-2-硝基乙烯合成路线 （共 10 条）
反应条件
ammonium acetate; acetic acid 6 h; Inert atmosphereSchlenk techniqueReflux;
参考文献
Park, Jung-Eun; Song, Chiman; Choi, Keehyun; Sim, Taebo; Moon, Bongjin; Roh, Eun Joo
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 20 p. 5515 - 5518
反应条件
ammonium acetate in nitromethane; acetic acid
参考文献
US5180733 A1, ;
US 5180733 A
反应条件
methanesulfonyl chloride; triethylamine in dichloromethane T=0 - 20°C;
参考文献
Journal of Organic Chemistry, , vol. 68, # 26 p. 9938 - 9947
反应条件
ammonium acetate in acetic acid T=60 - 65°C; Cyclization; condensation; nitration; 6 h; sonicated;
参考文献
Taylor, Edward C.; Liu, Bin; Wang, Wei
Journal of Organic Chemistry, 2000 , vol. 65, # 15 p. 4750 - 4752
反应条件
ammonium acetate in acetic acid T=60 - 65°C; Cyclization; condensation; nitration; 6 h; sonicated;
参考文献
Taylor, Edward C.; Liu, Bin; Wang, Wei
Journal of Organic Chemistry, 2000 , vol. 65, # 15 p. 4750 - 4752
反应条件
palladium (II) trifluoroacetate; silver(I) acetate in ethylene glycol dimethyl ether; dimethyl sulfoxide T=100°C; 24 h; GloveboxSchlenk techniqueInert atmosphere; Overall yield = 47 percent; regioselective reaction;
参考文献
Organic Letters, , vol. 15, # 7 p. 1718 - 1721
反应条件
1: aq. NaOH / ethanol / 65 h / 38 °C 2: CH3SO2Cl; Et3N / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 26 p. 9938 - 9947
反应条件
1: LiAlH4 / diethyl ether / Heating 2: H2SO4; AcOH / ethanol / 20 °C 3: HCl / ethanol / Heating View Scheme
参考文献
Bojarski, Andrzej J; Mokrosz, Maria J; Minol, Sijka Charakchieva; Koziol, Aneta; Wesolowska, Anna; Tatarczynska, Ewa; Klodzinska, Aleksandra; Chojnacka-Wojcik, Ewa
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 1 p. 87 - 95
反应条件
1: benzene-1,4-diol / toluene / Heating 2: H2 / Pd-C 3: (i) NaOEt, (ii) aq. HCl, NaHSO3 View Scheme
参考文献
Huitric,A.C. et al.
Journal of Organic Chemistry, 1962 , vol. 27, p. 715 - 719
反应条件
lithium aluminium tetrahydride in diethyl ether Heating;
参考文献
Bojarski, Andrzej J; Mokrosz, Maria J; Minol, Sijka Charakchieva; Koziol, Aneta; Wesolowska, Anna; Tatarczynska, Ewa; Klodzinska, Aleksandra; Chojnacka-Wojcik, Ewa
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 1 p. 87 - 95
