1-(5-硝基吡啶-2-基)乙酮合成路线 (共 5 条)
反应条件
ammonia in methanol T=100°C; 3 h; in sealed ampule;
参考文献
Sagitullina; Garkushenko; Vinokurova; Nyrkova; Atavin; Sagitullin
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 7 p. 1045 - 1049
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; potassium acetate / acetonitrile / 40 °C / Inert atmosphere 2: manganese(IV) oxide; potassium hydroxide / benzene / 3 h / 20 °C 3: sulfuric acid; mercury(II) diacetate; water / acetone / 2 h / Heating View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 46, # 12 p. 1830 - 1834
反应条件
1: manganese(IV) oxide; potassium hydroxide / benzene / 3 h / 20 °C 2: sulfuric acid; mercury(II) diacetate; water / acetone / 2 h / Heating View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 46, # 12 p. 1830 - 1834
反应条件
1: potassium hydroxide / benzene / 3 h / Reflux; Inert atmosphere 2: sulfuric acid; mercury(II) diacetate; water / acetone / 2 h / Heating View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 46, # 12 p. 1830 - 1834
反应条件
1: potassium fluoride / ethanol / 0.5 h 2: sulfuric acid; mercury(II) diacetate; water / acetone / 2 h / Heating View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 46, # 12 p. 1830 - 1834