3-羟基-3-苯基丁烷-2-酮合成路线 （共 33 条）
反应条件
sulfuric acid; water; mercury(II) oxide in tetrahydrofuran T=60°C; 2 h;
参考文献
Jirkovski, Ivo; Cayen, Mitchell, N.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 10 p. 1154 - 1156
反应条件
sulfuric acid; magnesium in tetrahydrofuran; toluene
参考文献
American Home Products Corporation (Del.)
Patent: US4704475 A1, 1987 ;
反应条件
Bi(NO3)3; water in benzene T=20°C; 2 h;
参考文献
Komatsu, Naoki; Taniguchi, Azusa; Wada, Shinobu; Suzuki, Hitomi
Advanced Synthesis and Catalysis, 2001 , vol. 343, # 5 p. 473 - 480
反应条件
polystyrene-supported N-heterocyclic carbene–silver complex T=40°C; P=37503.8 Torr; 24 h; Autoclave;
参考文献
Ca', Nicola Della; Gabriele, Bartolo; Ruffolo, Giuseppe; Veltri, Lucia; Zanetta, Tito; Costa, Mirco
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 133 - 146
反应条件
[rhodium(I)(carbonyl)2(acetylacetonate)] in ethylene glycol dimethyl ether; water T=80°C;
参考文献
Ganci, Gregory R.; Chisholm, John D.
Tetrahedron Letters, 2007 , vol. 48, # 47 p. 8266 - 8269
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 0.5 h; cooling;
参考文献
Kise, Naoki; Agui, Syun; Morimoto, Shinji; Ueda, Nasuo
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9407 - 9410
反应条件
[Rh(NCMe)2(cod)][BF4] in tetrahydrofuran T=60°C; 20 h;
参考文献
Oi, Shuichi; Moro, Mitsutoshi; Fukuhara, Hiroe; Kawanishi, Takanori; Inoue, Yoshio
Tetrahedron, 2003 , vol. 59, # 24 p. 4351 - 4361
反应条件
zinc dibromide in tetrahydrofuran 3 h;
参考文献
Katritzky, Alan R.; Bobrov, Sergey; Kirichenko, Kostyantyn; Ji, Yu
Journal of Organic Chemistry, 2004 , vol. 69, # 2 p. 303 - 308
反应条件
water; triethylamine in acetonitrile 0.5 h; Heating;
参考文献
Chudinov; Gashev; Firgang; Semenov
Russian Chemical Bulletin, 2007 , vol. 56, # 8 p. 1612 - 1616
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / -78 - -10 °C 1.2: tetrahydrofuran; hexane / -78 °C 2.1: Hg(ClO4)2; MeOH / 20 °C View Scheme
参考文献
Adlington, Robert M.; Baldwin, Jack E.; Bottaro, Jeffrey C.; Perry, Matthew W. D.
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 1040 - 1041
