3-(4-甲氧基苯甲酰基)丙酸合成路线 （共 71 条）
反应条件
AlCl3, aluminium chloride in 1,2-dichloro-ethane T=15 - 20°C; Friedel-Crafts Acylation; Cooling;
参考文献
Srinivas; Haricharan Raju; Acharyulu, Palle V. R.
Organic Process Research and Development, 2004 , vol. 8, # 2 p. 291 - 292
反应条件
barium dihydroxide in methanol T=20°C; 2 h;
参考文献
Anderson, Marc O.; Moser, Jamie; Sherrill, John; Guy, R. Kiplin
Synlett, 2004 , # 13 p. 2391 - 2393
反应条件
1: With succinic acid anhydride in tetrachloroethane, 1,1,2,2- T=0°C; 0.5 h; 2: With AlCl3, aluminium chloride in tetrachloroethane, 1,1,2,2- T=20°C; 36 h;
参考文献
WO2008/112368 A2, ;
Page/Page column 25-26 ;
反应条件
trifluoroacetic acid in dichloromethane 16 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 23, # 1 p. 375 - 381
反应条件
1: α-4-methoxyphenyl-α-(4-morpholino)acetonitrile With sodium hydride in N,N-dimethyl-formamide T=0°C; 0.5 h; 2: acrylic acid methyl ester in N,N-dimethyl-formamide T=0 - 20°C;
参考文献
Pawar; Waghmare; Lokhande
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 11 p. 2549 - 2551
反应条件
1: AlCl3; carbon disulfide 2: benzene / auf Siedetemperatur 3: aqueous KOH-solution <1 percent > / Erhitzen des Reaktionsprodukts mit 10prozentig.wss.Kalilauge View Scheme
参考文献
Journal of the American Chemical Society, , vol. 67, p. 286,290
反应条件
1: benzene / auf Siedetemperatur 2: aqueous KOH-solution <1 percent > / Erhitzen des Reaktionsprodukts mit 10prozentig.wss.Kalilauge View Scheme
参考文献
Journal of the American Chemical Society, , vol. 67, p. 286,290
反应条件
potassium hydroxide Erhitzen des Reaktionsprodukts mit 10prozentig.wss.Kalilauge;
参考文献
Journal of the American Chemical Society, , vol. 67, p. 286,290
反应条件
1: 38 percent / NaOMe / ethanol / 0.17 h / Heating 2: 32 percent / Ti(Oi-Pr)4; (+)-diethyl tartrate; t-BuOOH / CH2Cl2; decane / 114 h / -20 °C View Scheme
参考文献
Synthesis, , # 18 p. 3031 - 3036
反应条件
hydrogenchloride in 1,4-dioxane Heating;
参考文献
Gazzetta Chimica Italiana, , vol. 97, p. 654 - 664
