Alpha-甲基苯乙酸甲酯合成路线 （共 146 条）
反应条件
lithium perchlorate; methyl iodide Ambient temperatureanodic oxidation at constant current;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Katoh, Susumu; Fujita, Tetsuhiro; Kamada, Tohru
Tetrahedron Letters, 1989 , vol. 30, # 3 p. 371 - 374
反应条件
hydrogenchloride; triphenylphosphine; Pd(OAc)2 immobilized on montmorillonite in benzene T=125°C; P=31028.9 Torr; 24 h;
参考文献
Lee, Chul Woo; Alper, Howard
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 250 - 252
反应条件
1: potassium dimethoxy(phenyl)(trifluoromethyl)borate With chloro-trimethyl-silane in ethylene glycol dimethyl ether T=-20 - -10°C; 0.333333 h; Inert atmosphere; 2: ethyl α-diazopropanoate in ethylene glycol dimethyl ether T=-20 - 20°C; 13 h; Inert atmosphere;
参考文献
Elkin, Pavel K.; Levin, Vitalij V.; Dilman, Alexander D.; Struchkova, Marina I.; Belyakov, Pavel A.; Arkhipov, Dmitry E.; Korlyukov, Alexander A.; Tartakovsky, Vladimir A.
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5259 - 5263
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=160°C; P=15001.2 Torr; 0.2 h; microwave irradiation;
参考文献
Shieh, Wen-Chung; Dell, Steven; Repic, Oljan
Tetrahedron Letters, 2002 , vol. 43, # 32 p. 5607 - 5609
反应条件
1: styrene; carbon monoxide With hydrogenchloride; water; palladium diacetate; di-(1-adamantyl)-n-butylphosphine in 1,4-dioxane T=100°C; P=30003 Torr; 20 h; 2: diazomethyl-trimethyl-silane With methanol in 1,4-dioxane regioselective reaction;
参考文献
Neumann, Helfried; Brennfuehrer, Anne; Beller, Matthias
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 14-15 p. 2437 - 2442
反应条件
carbon tetrabromide T=20°C; 25 h; UV-irradiation;
参考文献
Lee, Shih-Yuan Adam; Yang, Hui-Chun; Su, Feng-Yih
Tetrahedron Letters, 2001 , vol. 42, # 2 p. 301 - 303
反应条件
sodium hypochlorite in acetic acid; acetone T=0°C; 10 h;
参考文献
Sugai, Saburo; Kodama, Takashi; Akaboshi, Sanya; Ikegami, Shiro
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 99 - 105
反应条件
tris(2,4-di-tert-butyl-phenyl) phosphite; hydrogen; [rhodium(I)(carbonyl)2(acetylacetonate)] in toluene T=100°C; P=9000.72 Torr; 40 h;
参考文献
Clarke, Matthew L.
Tetrahedron Letters, 2004 , vol. 45, # 21 p. 4043 - 4045
反应条件
5-chloro-2-hydroxy-benzoic acid; boric acid; tris(4-methylphenyl)-phosphine; palladium diacetate P=25857.4 Torr; 24 h; Heating;
参考文献
Vieira, Tiago O.; Green, Mike J.; Alper, Howard
Organic Letters, 2006 , vol. 8, # 26 p. 6143 - 6145
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; 16 h;
参考文献
Patil; Wadia
Synthetic Communications, 2002 , vol. 32, # 18 p. 2821 - 2827
