1: With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Alkylation; 24 h; Heating; 2: With sodium hydroxide; water Hydrolysis; 3: With water; dihydrogen peroxide; methyltrioxorhenium (VII) in dichloromethane T=20°C; Cyclization; 72 h; Title compound not separated from byproducts;
参考文献
Rudler, Henri; Parlier, Andree; Cantagrel, Frederic; Harris, Paul; Bellassoued, Moncef
Chemical Communications, 2000 , # 9 p. 771 - 772