3-甲基四氢吡喃-2,6-二酮合成路线 （共 6 条）
反应条件
hydrogen; magnesium sulfate; triethylamine; Ru2Cl4(DIOP)3 in toluene T=120°C; 20 h; other reagents: RuCl2(PPh3)3, RuCl2(ttp).; Product distribution;
参考文献
Ikariya, Takao; Osakada, Kohtaro; Ishii, Youichi; Osawa, Shoichi; Saburi, Masahiko; Yoshikawa, Sadao
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 897 - 898
参考文献
Berner; Leonardsen
Justus Liebigs Annalen der Chemie, 1939 , vol. 538, p. 27
Full Text Show Details
Berner; Leonardsen
Chem. Zentralbl., 1935 , vol. 106, # I p. 3781
反应条件
hydrogen; magnesium sulfate; triethylamine; Ru2Cl4(DIOP)3 in toluene
T=120°C; 20 h; other reagents: RuCl2(PPh3)3, RuCl2(ttp).; Product distribution;
参考文献
Ikariya, Takao; Osakada, Kohtaro; Ishii, Youichi; Osawa, Shoichi; Saburi, Masahiko; Yoshikawa, Sadao
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 897 - 898
反应条件
1: With ammonia in 1,4-dioxane; water
0.5 h;
2: T=230°C; 2 h;
参考文献
Pawlowski, Michal; Maurin, Jan K.; Leniewski, Andrzej; Wojtasiewicz, Krystyna; Czarnocki, Zbigniew
Heterocycles, 2005 , vol. 65, # 1 p. 9 - 22
反应条件
1: 3 h / Heating
2: oxalyl chloride / Ambient temperature
View Scheme
参考文献
Gruenfeld, Norbert; Stanton, James L.; Yuan, Andrew M.; Ebetino, Frank H.; Browne, Leslie J.; et al.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 9 p. 1277 - 1282
参考文献
Gruenfeld, Norbert; Stanton, James L.; Yuan, Andrew M.; Ebetino, Frank H.; Browne, Leslie J.; et al.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 9 p. 1277 - 1282
