3-烯丙基-2-羟基苯甲酸甲酯合成路线 (共 36 条)
反应条件
T=220°C; 1 h; Neat (no solvent);
参考文献
Bristol-Myers Squibb Company
Patent: EP1027043 B1, 2004 ;
Location in patent: Page/Page column 19 ;
反应条件
1: K2CO3 / acetone / Heating 2: 24 h / Heating View Scheme
参考文献
Meyers, A. I.; Reuman, Michael; Gabel, Richard A.
Journal of Organic Chemistry, 1981 , vol. 46, # 4 p. 783 - 788
反应条件
potassium carbonate in acetone 60 h;
参考文献
Meyers, A. I.; Reuman, Michael; Gabel, Richard A.
Journal of Organic Chemistry, 1981 , vol. 46, # 4 p. 783 - 788
反应条件
1: With potassium carbonate in acetone 16 h; Heating; 2: T=210°C; 3 h;
参考文献
Walker, Edward R.; Leung, Shing Y.; Barrett, Anthony G.M.
Tetrahedron Letters, 2005 , vol. 46, # 38 p. 6537 - 6540
反应条件
copper diacetate; manganese triacetate in acetic acid 30 h; Ambient temperature;
参考文献
Dombroski; Snider
Tetrahedron, 1992 , vol. 48, # 8 p. 1417 - 1426
反应条件
1: HCl (gas) / Heating 2: K2CO3 / acetone / Heating 3: N-methylpyrrolidinone / 7 h / Heating View Scheme
参考文献
Robertson, David W.; Lacefield, William B.; Bloomquist, William; Pfeifer, William; Simon, Richard L.; Cohen, Marlene L.
Journal of Medicinal Chemistry, 1992 , vol. 35, # 2 p. 310 - 319
反应条件
copper diacetate; manganese triacetate in acetic acid 38 h; Ambient temperature; Further byproducts given. Yields of byproduct given;
参考文献
Dombroski; Snider
Tetrahedron, 1992 , vol. 48, # 8 p. 1417 - 1426
反应条件
copper diacetate; manganese triacetate in acetic acid 38 h; Ambient temperatureother γ,γ-bis(allylic) acetoacetates; Mechanism;
参考文献
Dombroski; Snider
Tetrahedron, 1992 , vol. 48, # 8 p. 1417 - 1426
反应条件
1: aniline 2: NaOH-solution View Scheme
参考文献
Claisen
Justus Liebigs Annalen der Chemie, 1919 , vol. 418, p. 102
反应条件
1: aniline 2: NaOH-solution 3: ozone; acetic acid ester / Reduktion des Ozonids mit Zinkstaub und Eisessig View Scheme
参考文献
Claisen
Justus Liebigs Annalen der Chemie, 1919 , vol. 418, p. 102