1-甲基-2-苯基环丙烷合成路线 （共 19 条）
反应条件
lanthanum; iodine in tetrahydrofuran T=67°C; 5 h;
参考文献
Nishiyama, Yutaka; Tanimizu, Hana; Tomita, Tsuyoshi
Tetrahedron Letters, 2007 , vol. 48, # 36 p. 6405 - 6407
反应条件
tetrafluoroboric acid in dichloromethane T=-78°C;
参考文献
Journal of the American Chemical Society, , vol. 104, p. 6119
反应条件
1: diiodomethane With phosphoric acid diphenyl ester; diethylzinc in dichloromethane T=-10°C; 0.75 h; 2: trans-2-methylstyrene in dichloromethane T=-10 - 20°C; 15 h;
参考文献
Lacasse, Marie-Christine; Poulard, Cyril; Charette, Andre B.
Journal of the American Chemical Society, 2005 , vol. 127, # 36 p. 12440 - 12441
反应条件
lanthanum; iodine in tetrahydrofuran 5 h;
参考文献
Nishiyama, Yutaka; Tanimizu, Hana; Tomita, Tsuyoshi
Tetrahedron Letters, 2007 , vol. 48, # 36 p. 6405 - 6407
反应条件
1: Zn(CH2I)2 With ethylene glycol dimethyl ether; trichloroacetic acid in hexane; dichloromethane T=-15°C; Simmons-Smith Cyclopropanation; 1 h; Schlenk techniqueInert atmosphere; 2: cis-β-methylstyrene in hexane; dichloromethane T=-15 - 25°C; Simmons-Smith Cyclopropanation; 18 h; Schlenk techniqueInert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 34 p. 5588 - 5591
反应条件
1: Zn(CH2I)2 With ethylene glycol dimethyl ether; trichloroacetic acid in hexane; dichloromethane T=-15°C; Simmons-Smith Cyclopropanation; 1 h; Schlenk techniqueInert atmosphere; 2: trans-2-methylstyrene in hexane; dichloromethane T=-15 - 25°C; Simmons-Smith Cyclopropanation; 18 h; Schlenk techniqueInert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 34 p. 5588 - 5591
反应条件
water; Li-naphthalenide 1) THF, 1 min, room temperature; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 102, # 17 p. 5697 - 5699
反应条件
n-butyllithium; (cyclopropyl)2ZrCl2 in tetrahydrofuran T=-78 - 20°C;
参考文献
Tetrahedron Letters, , vol. 44, # 26 p. 4827 - 4829
反应条件
zinc copper; diethyl ether; iodine
参考文献
Journal of the American Chemical Society, , vol. 81, p. 4256,4258, 4262
Org. Synth. Coll. Vol., , vol. V, p. 855
反应条件
n-butyllithium; (cyclopropyl)2ZrCl2 in tetrahydrofuran T=-78 - 20°C;
参考文献
Gandon, Vincent; Laroche, Christophe; Szymoniak, Jan
Tetrahedron Letters, 2003 , vol. 44, # 26 p. 4827 - 4829
