D(+)-10-樟脑磺酸合成路线 （共 28 条）
反应条件
1: thionyl chloride / 1.) room temperature, 10 min, 2.) reflux, 1.5 h 2: 8.2 g / ammonia / CHCl3 / 0.67 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 20 p. 5412 - 5418
参考文献
Brungs; Danielmeier; Jakobi; Nothhelfer; Stahl; Zietlow; Steckhan
Journal de Chimie Physique et de Physico-Chimie Biologique, 1996 , vol. 93, # 4 p. 575 - 590
参考文献
Timmermans; Motiuk
Bulletin des Societes Chimiques Belges, 1932 , vol. 41, p. 399,408, 410
反应条件
Man unterwirft das entstehende Salz einer fraktionierten Krystallisation aus alkoholhaltigem Essigester;
参考文献
Barrowcliff; Tutin
Journal of the Chemical Society, 1909 , vol. 95, p. 1966
反应条件
1: 99 percent / thionyl chloride / DMF / 3 h / 20 °C 2: 100 percent / ammonium hydroxide / dioxane / 6 h / 20 - 95 °C 3: 66 percent / sodium borohydride / methanol; H2O / 1 h / 5 °C 4: 95 percent / sodium hydride / toluene / 16 h / 20 °C View Scheme
参考文献
Jung, Jae-Chul; Kache, Rajashaker; Vines, Kimberly K.; Zheng, Yan-Song; Bijoy, Panicker; Valluri, Muralikrishna; Avery, Mitchell A.
Journal of Organic Chemistry, 2004 , vol. 69, # 26 p. 9269 - 9284
反应条件
thionyl chloride; N,N-dimethyl-formamide T=20°C; 3 h;
参考文献
Jung, Jae-Chul; Kache, Rajashaker; Vines, Kimberly K.; Zheng, Yan-Song; Bijoy, Panicker; Valluri, Muralikrishna; Avery, Mitchell A.
Journal of Organic Chemistry, 2004 , vol. 69, # 26 p. 9269 - 9284
反应条件
1: thionyl chloride / 12 h / Reflux
2: triethylamine / dichloromethane / 5 h / 0 - 20 °C
View Scheme
参考文献
Lu, Chuanjun; Luo, Zonghua; Huang, Ling; Li, Xingshu
Tetrahedron Asymmetry, 2011 , vol. 22, # 7 p. 722 - 727
反应条件
1: SOCl2
2: NH3 / dioxane; H2O
3: 93 percent / NaBH4 / methanol; H2O
4: 85 percent / NaH / toluene; various solvent(s) / 2 h / 20 °C
View Scheme
参考文献
Liang, Bo; Carroll, Patrick J.; Joullie, Madeleine M.
Organic Letters, 2000 , vol. 2, # 26 p. 4157 - 4160
