D(+)-10-樟脑磺酸合成路线 （共 28 条）
反应条件
sulfuric acid; acetic anhydride
参考文献
Annali di Chimica Applicata, , vol. 30, p. 284,290
Organic Syntheses, , vol. 45, p. 12
反应条件
(-)-Brucine man zerlegt das ausscheideten Brucinsalz der <d-Campher>-β-sulfonsaeure mit Barytwasser;
参考文献
Chemische Berichte, , vol. 42, p. 3136
反应条件
Ba(ClO4)2 in methanol Resolution of racemate; SolventReagent/catalyst;
参考文献
Analytical Chemistry, , vol. 86, # 2 p. 1282 - 1290
反应条件
sulfuric acid; acetic anhydride die nach einiger Zeit auskrystallisierende Sulfonsaeure wird abgesaugt und mit Aether gewaschen;
参考文献
Bulletin de la Societe Chimique de France, , vol. <3>19, p. 125
参考文献
Tetrahedron: Asymmetry, , vol. 6, # 1 p. 43 - 46
参考文献
Journal of the American Chemical Society, , vol. 47, p. 1172
Organic Syntheses, , vol. 17, p. 80
参考文献
Journal of the Society of Chemical Industry, London, , vol. 47, p. 11 T
Chem. Zentralbl., , vol. 99, # I p. 2374
Journal of the Society of Chemical Industry, London, , vol. 44, # 497 p. 498 T
Chem. Zentralbl., , vol. 97, # I p. 914
参考文献
Ann. Chim. applic., , vol. 30, p. 284,288, 289
反应条件
1: (6R)-methyl-6-methyl-2-oxopiperidine-3-carboxylate With lithium aluminium tetrahydride in tetrahydrofuran; ethanol T=0 - 20°C; 2: (1S)-10-camphorsulfonic acid in tetrahydrofuran T=20°C;
参考文献
MERCK and CO., INC.; MERCK FROSST CANADA LTD.
Patent: WO2009/143033 A1, 2009 ;
Location in patent: Page/Page column 24-25 ;
WO 2009/143033 A1
反应条件
in tetrahydrofuran 1 h;
参考文献
Girardin, Melina; Ouellet, Stephane G.; Gauvreau, Danny; Moore, Jeffrey C.; Hughes, Greg; Devine, Paul N.; O'Shea, Paul D.; Campeau, Louis-Charles
Organic Process Research and Development, 2013 , vol. 17, # 1 p. 61 - 68
