2-甲基磺酰基-5-苯基嘧啶合成路线 （共 3 条）
反应条件
sodium methylate in methanol
参考文献
Frissen, A. E.; Marcelis, A. T. M.; Melger, W. C.; Plas, H. C. van der
Tetrahedron, 1989 , vol. 45, # 21 p. 6891 - 6900
反应条件
triethylsilane; palladium 10 on activated carbon in tetrahydrofuran T=0 - 20°C; 5 h; chemoselective reaction;
参考文献
Graham, Thomas H.; Liu, Wensheng; Shen, Dong-Ming
Organic Letters, 2011 , vol. 13, # 23 p. 6232 - 6235
反应条件
1: 30 percent / 30percent hydrogen peroxide / acetic acid / 6 h / 60 °C
2: 70 percent / N-methylpyrrolidone / 1.) room temp. 1 h, 2.) 50 deg C, 2 h, 3.) 60 deg C, 4 h
3: 71 percent / 15percent aq. sodium hydroxide / 0.5 h / Heating
View Scheme
参考文献
Mikhaleva, M. A.; Kolesnichenko, G. A.; Rubina, K. I.; Gol'dberg, Yu. Sh.; Savel'ev, V. A.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 3 p. 310 - 318
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 3 p. 380 - 388
