(4-氨基-3-硝基苯基)(苯基)甲酮合成路线 （共 12 条）
反应条件
hydrogen; platinum(IV) oxide
参考文献
Paquette,L.A.; Houser,R.W.
Journal of the American Chemical Society, 1971 , vol. 93, # 18 p. 4522 - 4526
反应条件
1: (photolysis) 2: KOtBu / 2-methyl-propan-2-ol 3: (photolysis) 4: (reduction) View Scheme
参考文献
Eaton,P.E.; Nyi,K.
Journal of the American Chemical Society, 1971 , vol. 93, p. 2786 - 2788
反应条件
1: KOtBu / 2-methyl-propan-2-ol 2: (photolysis) 3: (reduction) View Scheme
参考文献
Eaton,P.E.; Nyi,K.
Journal of the American Chemical Society, 1971 , vol. 93, p. 2786 - 2788
反应条件
water; platinum(IV) oxide in ethyl acetate
参考文献
Baldwin, John E.; Chang, Glenn E. C.
Journal of Organic Chemistry, 1982 , vol. 47, # 5 p. 848 - 851
反应条件
1: 41 percent / cupric sulfate / cyclohexane / 0.25 h / Heating 2: 74 percent / LiAlH4 / diethyl ether / 1.5 h / Heating 3: CrO3, pyridine / CH2Cl2 / 0.25 h 4: ethanol / Ambient temperature; overnight 5: NaH / tetrahydrofuran / 0.25 h 6: 1.5 h / 180 - 190 °C / 0.2 Torr 7: H2O / PtO2 / ethyl acetate View Scheme
参考文献
Baldwin, John E.; Chang, Glenn E. C.
Journal of Organic Chemistry, 1982 , vol. 47, # 5 p. 848 - 851
反应条件
1: CrO3, pyridine / CH2Cl2 / 0.25 h 2: ethanol / Ambient temperature; overnight 3: NaH / tetrahydrofuran / 0.25 h 4: 1.5 h / 180 - 190 °C / 0.2 Torr 5: H2O / PtO2 / ethyl acetate View Scheme
参考文献
Baldwin, John E.; Chang, Glenn E. C.
Journal of Organic Chemistry, 1982 , vol. 47, # 5 p. 848 - 851
反应条件
1: ethanol / Ambient temperature; overnight 2: NaH / tetrahydrofuran / 0.25 h 3: 1.5 h / 180 - 190 °C / 0.2 Torr 4: H2O / PtO2 / ethyl acetate View Scheme
参考文献
Baldwin, John E.; Chang, Glenn E. C.
Journal of Organic Chemistry, 1982 , vol. 47, # 5 p. 848 - 851
反应条件
1: 74 percent / LiAlH4 / diethyl ether / 1.5 h / Heating 2: CrO3, pyridine / CH2Cl2 / 0.25 h 3: ethanol / Ambient temperature; overnight 4: NaH / tetrahydrofuran / 0.25 h 5: 1.5 h / 180 - 190 °C / 0.2 Torr 6: H2O / PtO2 / ethyl acetate View Scheme
参考文献
Baldwin, John E.; Chang, Glenn E. C.
Journal of Organic Chemistry, 1982 , vol. 47, # 5 p. 848 - 851
反应条件
1: NaH / tetrahydrofuran / 0.25 h 2: 1.5 h / 180 - 190 °C / 0.2 Torr 3: H2O / PtO2 / ethyl acetate View Scheme
参考文献
Baldwin, John E.; Chang, Glenn E. C.
Journal of Organic Chemistry, 1982 , vol. 47, # 5 p. 848 - 851
反应条件
1: pentane / 12 h / 0 °C / Irradiation 2: 41 percent / cupric sulfate / cyclohexane / 0.25 h / Heating 3: 74 percent / LiAlH4 / diethyl ether / 1.5 h / Heating 4: CrO3, pyridine / CH2Cl2 / 0.25 h 5: ethanol / Ambient temperature; overnight 6: NaH / tetrahydrofuran / 0.25 h 7: 1.5 h / 180 - 190 °C / 0.2 Torr 8: H2O / PtO2 / ethyl acetate View Scheme
参考文献
Baldwin, John E.; Chang, Glenn E. C.
Journal of Organic Chemistry, 1982 , vol. 47, # 5 p. 848 - 851
