1,2,3,4,5-五苯基-1′-(二叔丁基膦)二茂铁合成路线 (共 4 条)
反应条件
sodium t-butanolate; palladium diacetate in chlorobenzene Pd acetate, Fe complex and NaO-t-Bu (molar ratio 1:20:1) in PhCl heatedat 110°C;
参考文献
Shelby; Kataoka; Mann; Hartwig
Journal of the American Chemical Society, 2000 , vol. 122, # 43 p. 10718 - 10719
反应条件
sodium t-butanolate in further solvent(s) react. of Fe and Pd complexes (molar ratio 1.1:1) and PhBr in the presence of NaO-t-Bu; not isolated; detd. by (1)H and (31)P NMR spectra;
参考文献
Journal of the American Chemical Society, , vol. 122, # 43 p. 10718 - 10719
反应条件
sodium t-butanolate in further solvent(s) react. of Fe and Pd complexes (molar ratio 1.1:1) and PhBr in the presence of NaO-t-Bu; treated with PCy3; not isolated; detd. by (1)H and (31)P NMR spectra;
参考文献
Journal of the American Chemical Society, , vol. 122, # 43 p. 10718 - 10719
反应条件
in not given 20-fold excess of Fe complex; 70°C, 1 h;
参考文献
Shelby; Kataoka; Mann; Hartwig
Journal of the American Chemical Society, 2000 , vol. 122, # 43 p. 10718 - 10719