反应条件
1: tetrakis(triphenylphosphine) palladium(0); K3PO4*7H2O / tetrahydrofuran / 12 h / 100 °C / |Inert atmosphere; |Schlenk technique 2: tetrahydrofuran / 1 h / 0 - 20 °C / |Inert atmosphere; |Schlenk technique 3: trichlorophosphate; triethylamine / tetrahydrofuran / 3 h / 0 °C / |Inert atmosphere; |Cooling with ice; |Schlenk technique View Scheme
参考文献
Liu, Jie; Fan, Chao; Yin, Hongyu; Qin, Chu; Zhang, Guoting; Zhang, Xu; Yi, Hong; Lei, Aiwen
Chemical Communications, 2014 , vol. 50, # 17 p. 2145 - 2147
