1,7-偶氮-15-冠-5合成路线 （共 17 条）
反应条件
hydrogen; 10 palladium on active carbon in ethanol T=25°C; P=3620.04 Torr; 24 h;
参考文献
Gatto, Vincent J.; Arnold, Kristin A.; Viscariello, Anthony M.; Miller, Steven R.; Morgan, Charles R.; Gokel, George W.
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5373 - 5384
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 8 h; Heating;
参考文献
Jurczak, Janusz; Kasprzyk, Stanislaw; Salanski, Piotr; Stankiewicz, Tomasz
Journal of the Chemical Society, Chemical Communications, 1991 , # 14 p. 956 - 957
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 20 h; Heating;
参考文献
Luk'yanenko, N.G.; Basok, S.S.; Filonova, L.K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 1562 - 1571
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1731 - 1742
反应条件
1: 80 percent / tetrabutylammonium iodide, sodium hydroxide (50 percent) / toluene; H2O / 9 h / Heating 2: 88 percent / lithium aluminum hydride / tetrahydrofuran / 20 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 24, p. 1562 - 1571
Zhurnal Organicheskoi Khimii, , vol. 24, # 8 p. 1731 - 1742
反应条件
1: 72 percent / Na2CO3, NaI / acetonitrile / 19 h / Heating 2: 91 percent / H2 / 10 Pd/C / ethanol / 24 h / 25 °C / 3620.04 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 26 p. 5373 - 5384
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 24 h; Heating;
参考文献
Jurczak, Janusz; Kasprzyk, Stanislaw; Salanski, Piotr; Stankiewicz, Tomasz
Journal of the Chemical Society, Chemical Communications, 1991 , # 14 p. 956 - 957
反应条件
sodium hydroxide; p-toluenesulfonyl chloride in 1,4-dioxane 3 h;
参考文献
Maeda; Furuyoshi; Nakatsuji; Okahara
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 10 p. 3073 - 3077
反应条件
1: 60 percent / methanol / 168 h / 25 °C / 750.06 Torr 2: 85 percent / lithium aluminium hydride (LAH) / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 14 p. 956 - 957
反应条件
sodium carbonate in acetonitrile 48 h; Heating;
参考文献
Krakowiak, Krzysztof E.; Maas, Garren E.; Bradshaw, Jerald S.; Hathaway, Jon K.; Izatt, Reed M.
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 1 p. 179 - 182
反应条件
1: 82 percent / lithium aluminum hydride / tetrahydrofuran / 10 h / Heating 2: 60 percent / toluene / 1.)0 deg C, 7 h 2.)overnight 3: 85 percent / lithium aluminum hydride / tetrahydrofuran / 8 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 18, p. 297 - 302
