外消旋2,4-二甲氧基-6-[[(三氟甲基)磺酰基]氧基]苯甲酸1-甲基-5-氧代-9-癸烯-1-基酯合成路线 （共 6 条）
反应条件
in pyridine; dichloromethane T=0°C; trifluoromethylsulfonylation; 3 h;
参考文献
Furstner; Thiel; Kindler; Bartkowska
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7990 - 7995
反应条件
1: 64 percent / PPh3; DEAD / diethyl ether / 3 h / 20 °C 2: 92 percent / CH2Cl2; pyridine / 3 h / 0 °C View Scheme
参考文献
Furstner; Thiel; Kindler; Bartkowska
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7990 - 7995
反应条件
1: 77 percent / diethyl ether; tetrahydrofuran / -78 - 20 °C 2: 64 percent / PPh3; DEAD / diethyl ether / 3 h / 20 °C 3: 92 percent / CH2Cl2; pyridine / 3 h / 0 °C View Scheme
参考文献
Furstner; Thiel; Kindler; Bartkowska
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7990 - 7995
反应条件
1: 77 percent / diethyl ether; tetrahydrofuran / -78 - 20 °C 2: 64 percent / PPh3; DEAD / diethyl ether / 3 h / 20 °C 3: 92 percent / CH2Cl2; pyridine / 3 h / 0 °C View Scheme
参考文献
Furstner; Thiel; Kindler; Bartkowska
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7990 - 7995
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine; lithium chloride in N,N-dimethyl-formamide T=90°C; Heck reaction; P=41254.1 Torr; 20 h;
参考文献
Furstner; Thiel; Kindler; Bartkowska
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7990 - 7995
反应条件
bis-triphenylphosphine-palladium(II) chloride; lithium chloride in N,N-dimethyl-formamide T=20°C; vinylation; 14 h;
参考文献
Furstner; Thiel; Kindler; Bartkowska
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7990 - 7995
