5-甲基四氢吡喃-2-酮合成路线 （共 17 条）
反应条件
pyridine; palladium diacetate in toluene T=80°C; Molecular sieve;
参考文献
Takeda, Kazutaka; Toyota, Masahiro
Tetrahedron Letters, 2011 , vol. 52, # 44 p. 5872 - 5875
反应条件
3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid in dichloromethane 1 h; 0 deg C to room temperature;
参考文献
Koch, Stacie S. Canan; Chamberlin, A. Richard
Synthetic Communications, 1989 , vol. 19, # 5and6 p. 829 - 834
反应条件
sodium hydroxide in methanol 2.5 h; Heating;
参考文献
Archibald, Sarah C.; Barden, David J.; Bazin, Jerome F.Y.; Fleming, Ian; Foster, Colin F.; Mandal, Ajay K.; Mandal, Amit K.; Parker, David; Takaki, Ken; Ware, Anne C.; Williams, Anne R.B.; Zwicky, Anna B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 7 p. 1051 - 1064
反应条件
potassium permanganate; iron(III) chloride in acetone T=-78 - 20°C; 15 h;
参考文献
Lai, Sheng; Lee, Donald G.
Tetrahedron, 2002 , vol. 58, # 49 p. 9879 - 9887
反应条件
dihydrogen peroxide; 1-n-butyl-3-methylimidazolium tetrafluoroborate; methyltrioxorhenium (VII) in water T=60°C; 24 h;
参考文献
Bernini, Roberta; Coratti, Antonietta; Fabrizi, Giancarlo; Goggiamani, Antonella
Tetrahedron Letters, 2003 , vol. 44, # 50 p. 8991 - 8994
反应条件
dihydrogen peroxide; polystyrene-bound phenylselenic acid in dichloromethane 103 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Taylor, Richard T.; Flood, Lawrence A.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5160 - 5164
反应条件
triethylamine; 4-phenylbut-3-en-2-one; Ru2Cl4(1,4-bis(diphenylphosphino)butane)3 in toluene T=140°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Ishii, Youichi; Osakada, Kohtaro; Ikariya, Takao; Saburi, Masahiko; Yoshikawa, Sadao
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2034 - 2039
反应条件
1,1,1-trifluoropropanone; methyl(trifluoromethyl)dioxirane in dichloromethane T=-10°C; 0.25 h; Yield given. Yields of byproduct given;
参考文献
Metsger, Leonid; Bittner, Shmuel
Tetrahedron, 2000 , vol. 56, # 13 p. 1905 - 1910
反应条件
potassium borohydride
参考文献
Archibald, Sarah C.; Barden, David J.; Bazin, Jerome F.Y.; Fleming, Ian; Foster, Colin F.; Mandal, Ajay K.; Mandal, Amit K.; Parker, David; Takaki, Ken; Ware, Anne C.; Williams, Anne R.B.; Zwicky, Anna B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 7 p. 1051 - 1064
反应条件
hydrogen; magnesium sulfate; triethylamine; Ru2Cl4(DIOP)3 in toluene T=120°C; 20 h; other reagents: RuCl2(PPh3)3, RuCl2(ttp).; Product distribution;
参考文献
Ikariya, Takao; Osakada, Kohtaro; Ishii, Youichi; Osawa, Shoichi; Saburi, Masahiko; Yoshikawa, Sadao
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 897 - 898
