2,3,5,6-四甲氧基环己-2,5-二烯-1,4-二酮合成路线 （共 14 条）
反应条件
in methanol T=20 - 70°C; 12 h; Inert atmosphere;
参考文献
Ganesh; Satheshkumar; Balraj; Elango
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2013 , vol. 107, p. 156 - 166
参考文献
Aoyama, Yasuhiro; Asakawa, Masumi; Matsui, Yuichi; Ogoshi, Hisanobu
Journal of the American Chemical Society, 1991 , vol. 113, # 16 p. 6233 - 6240
反应条件
in methanol 0.5 h; Heating;
参考文献
Keegstra, Erik M. D.; Huisman, Bart-Hendrik; Paardekooper, Elizabeth M.; Hoogesteger, Frans J.; Zwikker, Jan W.; Jenneskens, Leonardus W.; Kooijman, Huub; Schouten, Arie; Veldman, Nora; Spek, Anthony L.
Journal of the Chemical Society. Perkin Transactions 2, 1996 , vol. 2, p. 229 - 240
反应条件
1: 61 percent / aq. HNO3 / ethanol / 3 h / Ambient temperature 2: 75 percent / Br2 / CHCl3 / 5 h / Ambient temperature 3: 41 percent / MeONa / 1.) r.t., 3 h, 2.) 60 deg C, 30 min View Scheme
参考文献
Bock, Hans; Nick, Sabine; Seitz, Wolfgang; Naether, Christian; Bats, Jan W.
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1996 , vol. 51, # 2 p. 153 - 171
反应条件
1: 75 percent / Br2 / CHCl3 / 5 h / Ambient temperature 2: 41 percent / MeONa / 1.) r.t., 3 h, 2.) 60 deg C, 30 min View Scheme
参考文献
Bock, Hans; Nick, Sabine; Seitz, Wolfgang; Naether, Christian; Bats, Jan W.
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1996 , vol. 51, # 2 p. 153 - 171
反应条件
sodium methylate 1.) r.t., 3 h, 2.) 60 deg C, 30 min;
参考文献
Bock, Hans; Nick, Sabine; Seitz, Wolfgang; Naether, Christian; Bats, Jan W.
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1996 , vol. 51, # 2 p. 153 - 171
反应条件
1: methanol / 12 h / 20 - 70 °C / |Inert atmosphere 2: methanol / 12 h / 20 - 70 °C / |Inert atmosphere View Scheme
参考文献
Ganesh; Satheshkumar; Balraj; Elango
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2013 , vol. 107, p. 156 - 166
参考文献
Robinson; Vasey
Journal of the Chemical Society, 1941 , p. 660
反应条件
methanol; diethyl ether
参考文献
Eistert; Bock
Chemische Berichte, 1959 , vol. 92, p. 1247,1256
参考文献
Wallenfels,K.; Friedrich,K.
Chemische Berichte, 1960 , vol. 93, p. 3070 - 3082
