反应条件
1: 90 percent / POCl3 2: 1.) bis(2,4-dinitrophenyl)diselenide, 80percent H2O2, 2.) KOH / 1.) CH2Cl2, H2O, 3 h, 2.) MeOH, 1 h 3: 97 percent / NaOH, TEBA / tetrahydrofuran / 4 h 4: 1.) 1.6 M BuLi / 1.) hexane, THF, 3 h, - 5 deg C, 2.) 1 h 5: 53 percent / NaOH, TEBA / tetrahydrofuran / Ambient temperature 6: 36 percent / silver(II) dipicolinate / benzene; H2O / 1.5 h / Ambient temperature View Scheme
参考文献
Syper, Ludwik; Kloc, Krystian; Mlochowski, Jacek
Journal fuer Praktische Chemie (Leipzig), 1985 , vol. 327, # 5 p. 808 - 822
