1: N-chloro-succinimide; palladium diacetate; sodium peroxodisulphate; trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 0.33 h / 90 °C / |Sealed tube 2: N-chloro-succinimide; palladium diacetate; trifluorormethanesulfonic acid; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) / 1,2-dichloro-ethane / 4 h / 90 °C / |Sealed tube View Scheme

sodium peroxodisulphate; N-chloro-succinimide; trifluorormethanesulfonic acid; palladium diacetate in 1,2-dichloro-ethane T=90°C; 0.333333 h; Sealed tube;

[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); trifluoroacetic acid; trifluoroacetic anhydride T=85°C; 1 h;