二苯并[a,e]环辛烯-5(6H)-酮合成路线 (共 5 条)
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-10°C; 3 h; Inert atmosphere;
参考文献
Mbua, Ngalle Eric; Guo, Jun; Wolfert, Margreet A.; Steet, Richard; Boons, Geert-Jan
ChemBioChem, 2011 , vol. 12, # 12 p. 1912 - 1921
反应条件
pyridine; chromium(VI) oxide
参考文献
Popescu, Angela; Istrati, Daniela; Draghici, Constantin; Banciu, Anca; Mihaiescu, Dan; Ciuculescu, Crinu; Britzchi, Alina; Banciu, Mircea D.
Revue Roumaine de Chimie, 2001 , vol. 46, # 4 p. 439 - 444
反应条件
1: NBS 2: (i) collidine, DMSO, (ii) H2O View Scheme
参考文献
Yates,P. et al.
Canadian Journal of Chemistry, 1970 , vol. 48, p. 788 - 795
反应条件
2: NBS 3: (i) collidine, DMSO, (ii) H2O View Scheme
参考文献
Yates,P. et al.
Canadian Journal of Chemistry, 1970 , vol. 48, p. 788 - 795
反应条件
1: 60 percent / 2,6-di-tert-butyl-4-methylpyridine / CH2Cl2 / 20 °C
2: 80 percent / t-BuOK / tetrahydrofuran / 0 °C
View Scheme
参考文献
Chaffins, Sterling; Brettreich, Michael; Wudl, Fred
Synthesis, 2002 , # 9 p. 1191 - 1194