in tetrahydrofuran addition of Mg (suspension in THF) at -20°C to 4-BrC5F4N in THF, warming to -10 and 0°C, stirring for 1 hour;;
参考文献
Chambers, R. D.; Hutchinson, J.; Musgrave, W. K. R.
Journal of the Chemical Society, 1965 , p. 5040 - 5045
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Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67