反应条件
in tetrahydrofuran; diethyl ether byproducts: CH3SCH2MgBr; under anaerobic conditions, in NMR tube; Sn compd., Mg compd. (molar ratio 1:1) in Et2O, SnMe4 (internal standard) and THF mixed; reacted for 12d; not isolated; monitored by (119)Sn NMR spectra; < 5percent conversion;
参考文献
Yousef, Rushdi I; Rueffer, Tobias; Schmidt, Harry; Steinborn, Dirk
Journal of Organometallic Chemistry, 2002 , vol. 655, # 1-2 p. 111 - 114
