3-(二乙基氨基)-2-甲基丙酸甲酯合成路线 （共 6 条）
反应条件
ES-SO3H*Pyridine in tetrahydrofuran T=20°C; Aza-Michael condensation; 1 h; solid phase reaction;
参考文献
Verma, Sanny; Jain, Suman L.; Sain, Bir
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 7 p. 2314 - 2318
参考文献
Kohjin Co., Ltd.
Patent: US5587515 A1, 1996 ;
参考文献
Bieber
Annales de Chimie (Cachan, France), 1954 , vol. <12>9, p. 674,676
→
338-81-81,1,2,2,3,3,3-七氟-N,N-二(1,1,2,2,2-五氟乙基)丙-1-胺+
反应条件
hydrogen fluoride T=7 - 8°C; 10.2667 h; electrochemical reaction; anodic current density of 3.5 A dm-2, a cell voltage of 6.0 V - 6.1 V;
参考文献
Journal of Fluorine Chemistry, , vol. 66, # 2 p. 193 - 202
参考文献
Ficini,J. et al.
Bulletin de la Societe Chimique de France, 1962 , p. 1219 - 1224
→
338-81-81,1,2,2,3,3,3-七氟-N,N-二(1,1,2,2,2-五氟乙基)丙-1-胺+
反应条件
hydrogen fluoride
T=7 - 8°C; 10.2667 h; electrochemical reaction; anodic current density of 3.5 A dm-2, a cell voltage of 6.0 V - 6.1 V;
参考文献
Abe, Takashi; Fukaya, Haruhiko; Hayashi, Eiji; Hayakawa, Yoshio; Nishida, Masakazu; Baba, Hajime
Journal of Fluorine Chemistry, 1994 , vol. 66, # 2 p. 193 - 202
