2,3,5,7-四苯基-21H,23H-卟吩锰(2+)盐(1:1)合成路线 （共 24 条）
反应条件
in 2-methyl tetrahydrofuran Irradiation (UV/VIS); photoredn. of the Mn(III) complex in MeTHF by irradiation with visible light (440-750 nm) at 25°C; not isolated; detn. by UV/VIS spectral change;
参考文献
Enikolopov, N. S.; Gryaznov, V. M.; Solov'eva, A. B.; Rish, I. G.; Zavodchenko, S. I.; Ermilova, M. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, p. 629 - 630
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , vol. 34, p. 688 - 689
反应条件
tert-butyl benzene in chlorobenzene at 25°C for 112 min; not isolated, detected by ESR;
参考文献
Smegal, John A.; Hill, Craig L.
Journal of the American Chemical Society, 1983 , vol. 105, # 11 p. 3515 - 3521
反应条件
in solid High Pressure; 2000 MPa at room temp.; extrd. (chloroform), chromy. (alumina); UV;
参考文献
Zhorin, V. A.; Nikiforov, G. A.; Khristyuk, A. L.; Enikolopyan, N. S.
Doklady Physical Chemistry (Translation of the physical chemistry section of Doklady Akademii Nauk), 1983 , vol. 271, p. 510 - 512
Doklady Akademii Nauk SSSR, 1983 , vol. 271, p. 650 - 652
反应条件
in solid byproducts: N2; heating, 250 ° C, 5h, 1E-3 to 1E-5 Torr; chromy. (Al2O3, CH2Cl2, 30percent EtOH-C6H6), recrystn. (C6H6-hexane), drying (150 ° C, vac.), elem. anal.;
参考文献
Yamamoto, Yuichi; Imamura, Taira; Suzuki, Toru; Fujimoto, Masatoshi
Chemistry Letters, 1988 , p. 261 - 262
反应条件
in solid matrix Irradiation (UV/VIS); photolysis (300 W Xe arc lamp); 10K and 198 K;;
参考文献
Suslick, Kenneth S.; Bautista, Jocelyn F.; Watson, Randall A.
Journal of the American Chemical Society, 1991 , vol. 113, # 16 p. 6111 - 6114
反应条件
in solid matrix Irradiation (UV/VIS); photolysis (300 W Xe arc lamp); 10K and 198 K; mechanism discussed;;
参考文献
Suslick, Kenneth S.; Bautista, Jocelyn F.; Watson, Randall A.
Journal of the American Chemical Society, 1991 , vol. 113, # 16 p. 6111 - 6114
反应条件
in solid matrix Irradiation (UV/VIS); photolysis (300 W Xe arc lamp); 10K and 198 K; mechanism discussed;;
参考文献
Suslick, Kenneth S.; Bautista, Jocelyn F.; Watson, Randall A.
Journal of the American Chemical Society, 1991 , vol. 113, # 16 p. 6111 - 6114
反应条件
in 2-methyl tetrahydrofuran other Radiation; photoredn. of the Mn(III) complex in MeTHF by (60)Co γ-irradiation with visible light (440-750 nm) at 25°C; not isolated; detn. by UV/VIS spectral change;
参考文献
Suzuki, T.; Imamura, T.; Sumiyoshi, T.; Katayama, M.; Fujimoto, M.
Inorganic Chemistry, 1990 , vol. 29, p. 1123 - 1129
反应条件
in further solvent(s) electron-pulse irradiation in 2-methyltetrahydrofuran at 17°C; identification by absorption spectroscopy;
参考文献
Jin, Takashi; Suzuki, Toru; Imamura, Taira; Fujimoto, Masatoshi
Inorganic Chemistry, 1987 , vol. 26, p. 1280 - 1285
反应条件
in 2-methyl tetrahydrofuran Irradiation (UV/VIS); photoredn. of the Mn(III) complex in MeTHF by irradiation with visible light (440-750 nm) at 25°C; not isolated; detn. by UV/VIS spectral change;
参考文献
Jin, Takashi; Suzuki, Toru; Imamura, Taira; Fujimoto, Masatoshi
Inorganic Chemistry, 1987 , vol. 26, p. 1280 - 1285
