2,6-双（氯甲基）吡啶合成路线 （共 30 条）
反应条件
thionyl chloride 4 h;
参考文献
Bailey, Neil A.; Fenton, David E.; Kitchen, Simon J.; Lilley, Terence H.; Williams, Mark G.; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1991 , # 4 p. 627 - 637
反应条件
1: NaBH4 / methanol 2: thionyl chloride / benzene View Scheme
参考文献
Journal of the American Chemical Society, , vol. 106, # 19 p. 5497 - 5505
反应条件
N-chloro-succinimide; meta-chloroperoxybenzoic acid in tetrachloromethane 24 h; Heating;
参考文献
Synthesis, , # 8 p. 676 - 679
反应条件
N-chloro-succinimide; dibenzoyl peroxide in tetrachloromethane 24 h; Reflux;
参考文献
Inorganic Chemistry, , vol. 51, # 4 p. 2325 - 2331
反应条件
1: sodium tetrahydroborate / ethanol / 7 h / 20 °C / |Reflux; |Inert atmosphere 2: thionyl chloride / 3 h / 0 °C / |Reflux; |Inert atmosphere View Scheme
参考文献
Dalton Transactions, , vol. 41, # 48 p. 14480 - 14483
反应条件
1: thionyl chloride / 5 h / 0 °C / |Reflux; |Inert atmosphere 2: sodium tetrahydroborate / ethanol / 7 h / 20 °C / |Reflux; |Inert atmosphere 3: thionyl chloride / 3 h / 0 °C / |Reflux; |Inert atmosphere View Scheme
参考文献
Dalton Transactions, , vol. 41, # 48 p. 14480 - 14483
反应条件
chlorine Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 16, # 1 p. 89 - 93
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 16, # 1 p. 105 - 110
反应条件
in methanol; dichloromethane; water Kinetics; addn. of Au-complex in dichloromethane to LiCl+HClO4 in methanol:water (95:5 v/v) at 25 °C; detected by UV;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , # 2 p. 307 - 314
反应条件
in methanol; dichloromethane; water Kinetics; addn. of Au-complex in dichloromethane to LiCl+HClO4 in methanol:water (95:5 v/v) at 25 °C; detected by UV;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , # 2 p. 307 - 314
反应条件
1: 68 percent / Bu4N(HSO4); aq. 50 percent NaOH / toluene / Heating 2: 90 percent / HCl gas; NaOH / dioxane / 20 °C View Scheme
参考文献
Chellini, Andrea; Pagliarin, Roberto; Giovenzanna, Giovanni B.; Palmisano, Giovanni; Sisti, Massimo
Helvetica Chimica Acta, 2000 , vol. 83, # 4 p. 793 - 800
