3,5-二甲基-4-氨基苯酚合成路线 (共 32 条)
反应条件
1: With hydrogenchloride; sodium hydroxide; sodium nitrite in water T=0°C; 1 h; 2: With sodium tetrathionate in water T=20 - 75°C;
参考文献
Sumitomo Pharmaceuticals Company, Limited
Patent: EP1403255 A1, 2004 ;
Location in patent: Page 170 ;
EP 1403255 A1
反应条件
palladium on carbon; hydrogen in ethyl acetate P=750.075 Torr; 2 h;
参考文献
Schmidt, Bernd; Berger, Rene; Kelling, Alexandra; Schilde, Uwe
Chemistry - A European Journal, 2011 , vol. 17, # 25 p. 7032 - 7040
反应条件
perchloric acid; water T=40°C;
参考文献
Fishbein, James C.; McClelland, Robert A.
Journal of the American Chemical Society, 1987 , vol. 109, # 9 p. 2824 - 2825
反应条件
sodium dithionite; ethanol
参考文献
Journal of the American Chemical Society, , vol. 63, p. 1036,1040
反应条件
sulfuric acid in ethanol T=90°C; (electrochemical reduction);
参考文献
Bulletin de la Societe Chimique de France, , p. 1848 - 1858
反应条件
sodium dithionite; 4-sulfobenzenediazonium cation 1.) 1 h, 2.) 65 deg C to 70 deg C; Yield given. Multistep reaction;
参考文献
Journal of Medicinal Chemistry, , vol. 23, # 11 p. 1153 - 1158
反应条件
sodium dithionite T=65°C;
参考文献
Mutation Research - Genetic Toxicology and Environmental Mutagenesis, , vol. 395, # 2-3 p. 159 - 171
反应条件
und anschliessenden Reduktion mit Na2S2O4;
参考文献
Journal of the American Chemical Society, , vol. 76, p. 4983
反应条件
sodium hydroxide; sodium dithionite
参考文献
Journal of the Society of Chemical Industry, London, , vol. 49, p. 469 T, 472 T
反应条件
1: K2SO5 View Scheme
参考文献
Journal of the Chemical Society, , p. 4198