2-碘-9h-芴-9-酮合成路线 （共 10 条）
反应条件
sulfuric acid; iodine; periodic acid in water; acetic acid T=20 - 60°C; 21.5 h;
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/40110 A1, 2005 ;
Location in patent: Page/Page column 88-89 ;
反应条件
sodium dichromate in acetic acid 4 h; Heating;
参考文献
Hauser, A.; Thurner, J.-U.; Hinzmann, B.
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 3 p. 367 - 378
反应条件
1: With sulfuric acid; sodium nitrite 2: With potassium iodide
参考文献
Ahmed, Saleh Abdel-Mgeed; Al-Raqa, Shaya Y.
Journal of Physical Organic Chemistry, 2011 , vol. 24, # 3 p. 173 - 184
反应条件
tris(trifluoroacetoxy)-λ3-iodane in dichloromethane 3 h; Ambient temperature;
参考文献
Fukuyama, Norihiro; Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 12 p. 4363 - 4368
参考文献
Korczynski; Karlowska; Kierzek
Bulletin de la Societe Chimique de France, 1927 , vol. <4> 41, p. 69
Full Text Show Details
Chanussot
Anales de la Asociacion Quimica Argentina (1921-2001), vol. 15, p. 8
反应条件
2-aminopyridine; Cu(NO3)2*3H2O; oxygen; silver carbonate in N,N-dimethyl-formamide T=150°C; 24 h; Schlenk technique;
参考文献
Pawar, Amit B.; Chang, Sukbok
Chemical Communications, 2014 , vol. 50, # 4 p. 448 - 450
参考文献
Hinzmann, B.; Thurner, J.-U.; Stoesser, R.; Knoll, B.; Tomaschewski, G.
Zeitschrift fuer Chemie (Stuttgart, Germany), 1985 , vol. 25, # 8 p. 301
反应条件
anhydrous ammonium carbonate; hydrogenchloride; potassium cyanide in sodium hydroxide; ethanol
参考文献
Alcon Laboratories, Inc.
Patent: US4540700 A1, 1985 ;
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine in tetrahydrofuran
Sonogashira coupling; 4 h;
参考文献
Ahmed, Saleh A.; Al-Raqa, Shaya Y.
Monatshefte fur Chemie, 2010 , vol. 141, # 3 p. 357 - 372
反应条件
1: copper-powder / 225 - 230 °C
2: N2H4
View Scheme
参考文献
Barnett et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 4583,4585
