4-硝基-3,5-二甲基苯甲酸合成路线 （共 27 条）
反应条件
chromium(VI) oxide; acetic acid T=20°C; 12.5 h;
参考文献
Ieda, Naoya; Nakagawa, Hidehiko; Horinouchi, Taeko; Peng, Tao; Yang, Dan; Tsumoto, Hiroki; Suzuki, Takayoshi; Fukuhara, Kiyoshi; Miyata, Naoki
Chemical Communications, 2011 , vol. 47, # 22 p. 6449 - 6451
反应条件
in water; acetic acid
反应条件
chromium(VI) oxide; sulfuric acid; acetic acid 0.5 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of Medicinal Chemistry, , vol. 47, # 8 p. 1969 - 1986
参考文献
Justus Liebigs Annalen der Chemie, , vol. 141, p. 134
Justus Liebigs Annalen der Chemie, , vol. 193, p. 162,166
Justus Liebigs Annalen der Chemie, , vol. 147, p. 50
反应条件
nitric acid Trennung der Saeuren in Form ihrer Bariumsalzes unterhalb 15grad;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 193, p. 162,166
Chemische Berichte, , vol. 34, p. 29
反应条件
1: diluted nitric acid 2: fuming nitric acid / Trennung der Saeuren in Form ihrer Bariumsalzes unterhalb 15grad View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 193, p. 162,166
参考文献
Justus Liebigs Annalen der Chemie, , vol. 193, p. 162,166
Chemische Berichte, , vol. 34, p. 29
参考文献
Justus Liebigs Annalen der Chemie, , vol. 141, p. 134
Justus Liebigs Annalen der Chemie, , vol. 147, p. 296
反应条件
1: (i) PCl5, (ii) aq. NH3 2: aq. NaOH, Br2 3: (i) aq. HCl, NaNO2, (ii) HPF6 View Scheme
参考文献
Dewar,M.J.S.; Takeuchi,Y.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 390 - 394
反应条件
hydrogenchloride; sodium carbonate; zinc in water T=30°C; 0.833333 h;
参考文献
Favre-Besse, Franck-Cyril; Poirel, Odile; Bersot, Tiphaine; Kim-Grellier, Elodie; Daumas, Stephanie; El Mestikawy, Salah; Acher, Francine C.; Pietrancosta, Nicolas
European Journal of Medicinal Chemistry, 2014 , vol. 78, p. 236 - 247
