N,N-二乙基-1,1,2,3,3,3-六氟丙胺合成路线 （共 16 条）
反应条件
n-butyllithium; triethylamine in N,N-dimethyl-formamide T=-5°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 28, # 32 p. 3699 - 3702
反应条件
sodium hydride; triethylamine in N,N-dimethyl-formamide T=-5°C; 6 h;
参考文献
Tetrahedron Letters, , vol. 28, # 32 p. 3699 - 3702
反应条件
in diethyl ether Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 23, p. 383 - 388
反应条件
hydrogen fluoride 5-6 V, 2 A dm-2, 135 A h,; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 82, # 2 p. 143 - 150
反应条件
in dichloromethane T=2 - 20°C; 48 h; Inert atmosphere;
参考文献
Grieco, Liane M.; Halliday, Gary A.; Junk, Christopher P.; Lustig, Steven R.; Marshall, William J.; Petrov, Viacheslav A.
Journal of Fluorine Chemistry, 2011 , vol. 132, # 12 p. 1198 - 1206
参考文献
Ali, Majeid; Liu, Le-Ping; Hammond, Gerald B.; Xu, Bo
Tetrahedron Letters, 2009 , vol. 50, # 28 p. 4078 - 4080
反应条件
in dichloromethane 6 h; Ambient temperature;
参考文献
Watanabe, S.; Fujita, T.; Sakamoto, M.; Endo, H.
Journal of Fluorine Chemistry, 1988 , vol. 38, p. 243 - 248
反应条件
in dichloromethane 3 h; Ambient temperature;
参考文献
Watanabe, S.; Fujita, T.; Sakamoto, M.; Kuramochi, T.; Kitazume, T.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 361 - 372
反应条件
in tetrahydrofuran
T=40 - 50°C; 3 h;
参考文献
Watanabe, Shoji; Fujita, Tsutomu; Suga, Kyoichi; Nasuno, Ichiro
Synthesis, 1984 , # 1 p. 31 - 33
