perchloric acid in diethyl ether; water T=10 - 20°C; Large scale; SolventTemperatureTime;

perchloric acid in diethyl ether; water

1: methyl (methylthiomethyl)-sulfoxide With n-butyllithium in tetrahydrofuran T=-20°C; 3 h; 2: (((1,3-dibromopropan-2-yl)oxy)methyl)benzene in tetrahydrofuran T=-78 - 20°C; 3: With hydrogenchloride; water in diethyl ether 0.5 h; Heating / reflux;

1: 77 percent / n-BuLi / tetrahydrofuran / 1.) -70 degC, 2h, 2.) room temperature, 15.5h 2: 60 percent / 35percent HClO4 / diethyl ether / 25 h / Ambient temperature View Scheme

1: dimercury dichloride / 160 °C 2: n-butyllithium / tetrahydrofuran 3: hydrogenchloride / tetrahydrofuran View Scheme

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palladium